Single-crystal X-ray diffraction study of novel pyrazole chalcone derived from 1-phenyl-3-p-tolyl-1H-pyrazole-4-carbaldehyde

被引：0

作者：

Banpurkar, Anita R. ^{[1
]}

Wazalwar, Sachin S. ^{[1
]}

Perdih, Franc ^{[2
]}

机构：

[1] Rajiv Gandhi Coll Engn Res & Technol, Dept Appl Chem, Chandrapur 442403, India

[2] Univ Ljubljana, Fac Chem & Chem Technol, SI-1000 Ljubljana, Slovenia

来源：

INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY | 2020年 / 59卷 / 01期

关键词：

Microwave assisted pyrazole carbaldehyde; chalcone; acetophenone; single-crystal study; DERIVATIVES;

D O I：

暂无

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Novel pyrazole chalcone has been synthesized by reaction of phenyl-3-p-tolyl-1H-pyrazole-4-carbaldehyde and acetophenone by Claisen-Schmidt reaction in ethanol by microwave assisted method. It has been characterized by elemental analysis and spectroscopic (FTIR, H-1 NMR and MS) studies. Crystal structure of the compound has been determined using single-crystal X-ray diffraction. Hydrogen-bonded chain is formed by C-H center dot center dot center dot O bonding enhanced by C-H...pi interaction. Adjacent chains are connected through the pi...pi interactions.

引用

页码：143 / 146

页数：4

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