Single-crystal X-ray diffraction study of novel pyrazole chalcone derived from 1-phenyl-3-p-tolyl-1H-pyrazole-4-carbaldehyde

被引：0
|
作者：
Banpurkar, Anita R. [1 ]
Wazalwar, Sachin S. [1 ]
Perdih, Franc [2 ]
机构：
[1] Rajiv Gandhi Coll Engn Res & Technol, Dept Appl Chem, Chandrapur 442403, India
[2] Univ Ljubljana, Fac Chem & Chem Technol, SI-1000 Ljubljana, Slovenia
来源：
INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY | 2020年 / 59卷 / 01期
关键词：
Microwave assisted pyrazole carbaldehyde; chalcone; acetophenone; single-crystal study; DERIVATIVES;
D O I：
暂无
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Novel pyrazole chalcone has been synthesized by reaction of phenyl-3-p-tolyl-1H-pyrazole-4-carbaldehyde and acetophenone by Claisen-Schmidt reaction in ethanol by microwave assisted method. It has been characterized by elemental analysis and spectroscopic (FTIR, H-1 NMR and MS) studies. Crystal structure of the compound has been determined using single-crystal X-ray diffraction. Hydrogen-bonded chain is formed by C-H center dot center dot center dot O bonding enhanced by C-H...pi interaction. Adjacent chains are connected through the pi...pi interactions.
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页码：143 / 146
页数：4
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