Synthesis of hollow mesoporous silica spheres with radially aligned mesochannels and tunable textural properties

被引：23
|
作者：
Liu, Ruiping [1 ,2 ]
Wang, Chang-an [2 ]
机构：
[1] China Univ Min & Technol Beijing, Dept Mat Sci & Engn, Beijing 100083, Peoples R China
[2] Tsinghua Univ, State Key Lab New Ceram & Fine Proc, Sch Mat Sci & Engn, Beijing 100084, Peoples R China
来源：
CERAMICS INTERNATIONAL | 2015年 / 41卷 / 01期
基金：
中国国家自然科学基金;
关键词：
Carbon spheres; Hollow silica spheres; Mesochannels; Surface area; MOLECULAR-SIEVES; MORPHOLOGICAL CONTROL; SPHERICAL SILICA; ADSORPTION; CHANNELS;
D O I：
10.1016/j.ceramint.2014.09.035
中图分类号：
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号：
0805 ; 080502 ;
摘要：
Hollow mesoporous silica spheres with radially aligned mesochannels were fabricated successfully by combining hard and soft templating methods. The microstructure, textural properties and the structure regulation approach of the hollow spheres were investigated. The results show that the hollow spheres are perfectly spherical, monodisperse, and present ordered mesochannels with pore size of similar to 2.20 nm, high specific surface area and high pore volume. The textural properties of the hollow mesoporous silica spheres can be tuned by adjusting the alkali-treatment process of the carbon spheres and the concentration of the inorganic source. (C) 2014 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
引用
收藏
页码：1101 / 1106
页数：6
相关论文
共 50 条
  • [21] Preparation of mesoporous 1,2-ethylene-silica hollow spheres with tunable wall thickness
    Yan, Zhuojun
    Wang, Sibing
    Wu, Limin
    Li, Yi
    Li, Baozong
    Zhu, Guangshan
    Yang, Yonggang
    MATERIALS LETTERS, 2012, 78 : 14 - 17
  • [22] Synthesis and Characterization of Hollow Mesoporous Silica Spheres and Studying the Load and Release of Dexamethasone
    Al Roaya, M. Amin
    Manteghi, F.
    Haghverdi, M.
    SILICON, 2019, 11 (03) : 1401 - 1411
  • [23] Aerosol assisted synthesis of silica/phenolic resin composite mesoporous hollow spheres
    Yu, Xianglin
    Ding, Shujiang
    Meng, Zhaokai
    Liu, Jiguang
    Qu, Xiaozhong
    Lu, Yunfeng
    Yang, Zhenzhong
    COLLOID AND POLYMER SCIENCE, 2008, 286 (12) : 1361 - 1368
  • [24] Aerosol assisted synthesis of silica/phenolic resin composite mesoporous hollow spheres
    Xianglin Yu
    Shujiang Ding
    Zhaokai Meng
    Jiguang Liu
    Xiaozhong Qu
    Yunfeng Lu
    Zhenzhong Yang
    Colloid and Polymer Science, 2008, 286 : 1361 - 1368
  • [25] Synthesis and Characterization of Hollow Mesoporous Silica Spheres and Studying the Load and Release of Dexamethasone
    M. Amin Al Roaya
    F. Manteghi
    M. Haghverdi
    Silicon, 2019, 11 : 1401 - 1411
  • [26] Preparation of mesoporous silica films with fully aligned large mesochannels using nonionic surfactants
    Miyata, H
    Noma, T
    Watanabe, M
    Kuroda, K
    CHEMISTRY OF MATERIALS, 2002, 14 (02) : 766 - 772
  • [27] Sandwich-Type Nanocomposite of Reduced Graphene Oxide and Periodic Mesoporous Silica with Vertically Aligned Mesochannels of Tunable Pore Depth and Size
    Wang, Zheng-Ming
    Peng, Wenqin
    Takenaka, Yoshiko
    Yoshizawa, Noriko
    Kosuge, Katsunori
    Wang, Wendong
    Ozin, Geoffrey A.
    ADVANCED FUNCTIONAL MATERIALS, 2017, 27 (47)
  • [28] Catalytic Characterization of Mesoporous Ti–Silica Hollow Spheres
    M. Baca
    W. J. Li
    P. Du
    G. Mul
    J. A. Moulijn
    M.-O. Coppens
    Catalysis Letters, 2006, 109 : 207 - 210
  • [29] Control of Periodicity in Mesoporous Silica Films with Aligned Mesochannels Prepared by a Sol-Gel Process
    Komoto, Atsushi
    Kubo, Wataru
    Miyata, Hirokatsu
    CHEMISTRY LETTERS, 2012, 41 (07) : 741 - 743
  • [30] Synthesis and Characterization of Hollow Silica Spheres
    Gorsd, Marina N.
    Pizzio, Luis R.
    Blanco, Mirta N.
    INTERNATIONAL CONGRESS OF SCIENCE AND TECHNOLOGY OF METALLURGY AND MATERIALS, SAM - CONAMET 2013, 2015, 8 : 567 - 576
12345