A new and facile synthesis of methyl 3-amino-4,5,6,7-tetrahydrobenzo[b]thiophene-2-carboxylate

被引：4
|
作者：
Tenora, Lukas [1 ]
Buchlovic, Marian [1 ]
Man, Stanislav [1 ]
Potacek, Milan [1 ]
机构：
[1] Masaryk Univ, Dept Chem, CS-61137 Brno, Czech Republic
来源：
TETRAHEDRON LETTERS | 2011年 / 52卷 / 03期
关键词：
ENAMINES;
D O I：
10.1016/j.tetlet.2010.11.076
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A four-step synthesis of methyl 3-amino-4,5,6,7-tetrahydrobenzo[b]thiophene-2-carboxylate from commercially available starting materials is presented. (c) 2010 Elsevier Ltd. All rights reserved.
引用
收藏
页码：401 / 403
页数：3
相关论文
共 50 条
  • [21] 2-Salicylideneamino-4,5,6,7-tetrahydrobenzo[b]-thiophene-3-carbo nitril e
    Acta Crystallogr Sect C Cryst Struct Commun, pt 4 (529):
  • [22] The reaction of 2-amino-3-cyano-4,5,6,7-tetrahydrobenzo[b]-thiophene with diethyl malonate:: Synthesis of coumarin, pyridine, and thiazole derivatives
    Mohareb, RM
    El-Omran, FA
    Ho, JZ
    HETEROATOM CHEMISTRY, 2001, 12 (03) : 168 - 175
  • [23] SYNTHESIS OF 2-AMINO-3-CARBETHOXY-4,5,6,7-TETRAHYDROBENZO[B]SELENOPHENE, AND SOME OF ITS TRANSFORMATIONS
    KHRIPAK, SM
    DOBOSH, AA
    SMOLANKA, IV
    MIKITCHI.AS
    KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 1973, (03): : 326 - 328
  • [24] SYNTHESIS AND STRUCTURE OF 7-OXO-4,5,6,7-TETRAHYDROBENZO[B]THIOPHENE AND 7-HYDROXYBENZO[B]THIOPHENE
    KHARIZOMENOVA, IA
    KAPUSTINA, MV
    GRINEV, AN
    SHEINKER, YN
    ALEKSEEVA, LM
    KULESHOVA, YF
    KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 1984, (12): : 1626 - 1629
  • [25] 2-(2-Nitroanilino)-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carbonitrile
    Mendonca Junior, Francisco J. B.
    de Lima, Maria do Carmo A.
    Galdino, Suely L.
    Pitta, Ivan R.
    de Simone, Carlos A.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O2543 - U323
  • [26] Reaction of ethyl 2-diazo-4,5,6,7-tetrahydrobenzo[b] thiophene 3-carboxylate with benzoyl acetonitrile: Synthesis of pyridazines, pyrimidines and their fused derivatives
    Mohareb, RM
    Mohamed, MH
    Wardakhan, WW
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2000, 167 : 29 - 45
  • [27] Reaction of ethyl 2-diazo-4,5,6,7-tetrahydrobenzo [b]thiophene-3-carboxylate with 3-iminobutyronitrile:: Synthesis of pyridazines, thiophenes, and their fused derivatives
    Mohareb, RM
    Manhi, FM
    HETEROATOM CHEMISTRY, 2000, 11 (06) : 403 - 412
  • [28] Reaction of ethyl 2-diazo-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate with 3-iminobutyronitrile: Synthesis of pyridazines, thiophenes, and their fused derivatives
    Mohareb, Rafat M.
    Manhi, Fatma M.
    2000, John Wiley & Sons Inc, United States (11)
  • [29] Crystal structure of 3-benzoyl-2-[(5-bromo-2-hydroxy-3-methoxybenzylidene)amino]-4,5,6,7-tetrahydrobenzo[b]thiophene
    Kaur, Manpreet
    Jasinski, Jerry P.
    Yathirajan, H. S.
    Glidewell, Christopher
    Byrappa, K.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : 176 - +
  • [30] Synthesis and Chemical Reactivity of New Azaenamines Incorporated the 4,5,6,7-Tetrahydrobenzo[b]thiophene Moiety: 3+3 Atom Combination
    Abdelhamid, Ismail Abdelshafy
    Darwish, Elham Sayed
    Nasra, Miead Adel
    Abdel-Gallil, Fathy Mohamed
    Fleita, Daisy Hanna
    SYNTHESIS-STUTTGART, 2010, (07): : 1107 - 1112
12345