Mechanical properties and fracture toughness of organo-silicate glass (OSG) low-k dielectric thin films for microelectronic applications

被引:67
|
作者
Vella, JB [1 ]
Adhihetty, IS
Junker, K
Volinsky, AA
机构
[1] Motorola Inc, DigitalDNA TM Labs, Proc & Mat Characterizat Lab, Tempe, AZ 85284 USA
[2] Motorola Inc, Adv Prod Res & Dev Lab, Digital DNA TM Labs, Austin, TX 78721 USA
关键词
adhesion; fracture toughness; low-k dielectrics; mechanical properties; thin films;
D O I
10.1023/A:1024944316369
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The integration of chemical vapor deposited organo-silicate glass (OSG) interlayer dielectrics (ILD) has challenged the IC industry to formulate new methods of metrology and characterization. The impact of nanoindentation to understand and screen for integrated circuit failure mechanisms that are mainly predicated upon OSG nano-porosity is discussed. Failure modes include poor mechanical strength, low material stiffness, and brittle fracture due to low cohesive and adhesive fracture toughness, a particular danger during chemical-mechanical polishing (CMP). By developing a methodology to predict failure modes, we are able to screen multiple candidate low-k materials. Nanoindentation measurements of elastic modulus, hardness, and fracture toughness and what they reveal about OSG porosity are discussed.
引用
收藏
页码:487 / 499
页数:13
相关论文
共 50 条
  • [11] Investigation of mechanical properties of black diamond™ (low-K) thin films for Cu/low-k interconnect applications
    Sekbar, V. N.
    Balakumar, S.
    Chai, T. C.
    Tay, Andrew A. O.
    EPTC 2006: 8TH ELECTRONIC PACKAGING TECHNOLOGY CONFERENCE, VOLS 1 AND 2, 2006, : 63 - 69
  • [12] Organofluoro silicate glass:: A dense low-k dielectric with superior materials properties
    Cheng, Y. L.
    Wang, Y. L.
    Juang, Yungder
    O'Neill, M. L.
    Lukas, A. S.
    Karwacki, E. J.
    NlcGuian, S. A.
    Tang, Allen
    Wu, C. L.
    JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS, 2008, 69 (2-3) : 518 - 522
  • [13] Dielectric properties of parylene AF4 as low-k material for microelectronic applications
    Kahouli, A.
    Sylvestre, A.
    Jomni, F.
    Andre, E.
    Garden, J-L
    Yangui, B.
    Berge, B.
    Legrand, J.
    THIN SOLID FILMS, 2012, 520 (07) : 2493 - 2497
  • [14] UV curing effects on glass structure and mechanical properties of organosilicate low-k thin films
    Gage, David M.
    Guyer, Eric P.
    Stebbins, Jonathan F.
    Cui, Zhenjiang
    Al-Bayati, Amir
    Demos, Alex
    MacWilliams, Kenneth P.
    Dauskardt, Reinhold H.
    PROCEEDINGS OF THE IEEE 2006 INTERNATIONAL INTERCONNECT TECHNOLOGY CONFERENCE, 2006, : 149 - +
  • [15] Determination of the hardness and elastic modulus of low-k thin films and their barrier layer for microelectronic applications
    Shen, L
    Zeng, KY
    Wang, YH
    Narayanan, B
    Kumar, R
    MICROELECTRONIC ENGINEERING, 2003, 70 (01) : 115 - 124
  • [16] Hydrogenation of Boron Carbon Nitride Thin Films for Low-k Dielectric Applications
    Nehate, Shraddha Dhanraj
    Sundaresh, Sreeram
    Peale, Robert
    Sundaram, Kalpathy B.
    ECS JOURNAL OF SOLID STATE SCIENCE AND TECHNOLOGY, 2021, 10 (09)
  • [17] Advanced metrology for rapid characterization of the thermal mechanical properties of low-k dielectric and copper thin films
    Lau, SH
    Tolentino, E
    Lim, Y
    Tolentino, E
    Koo, A
    JOURNAL OF ELECTRONIC MATERIALS, 2001, 30 (04) : 299 - 303
  • [18] Advanced metrology for rapid characterization of the thermal mechanical properties of low-k dielectric and copper thin films
    S. H. Lau
    Ellie Tolentino
    Yuen Lim
    Evangeline Tolentino
    Ann Koo
    Journal of Electronic Materials, 2001, 30 : 299 - 303
  • [19] Mechanical properties of surface modified silica low-k thin films
    Mhaisagar, Yogesh S.
    Joshi, Bhavana N.
    Mahajan, Ashok M.
    MICROELECTRONIC ENGINEERING, 2014, 114 : 112 - 116
  • [20] Mechanical property changes in porous low-k dielectric thin films during processing
    Stan, G.
    Gates, R. S.
    Kavuri, P.
    Torres, J.
    Michalak, D.
    Ege, C.
    Bielefeld, J.
    King, S. W.
    APPLIED PHYSICS LETTERS, 2014, 105 (15)