Rapid thermal processing chamber for in-situ x-ray diffraction

被引：16

作者：

Ahmad, Md Imteyaz ^{[1
]}

Van Campen, Douglas G. ^{[1
]}

Fields, Jeremy D. ^{[2
]}

Yu, Jiafan ^{[1
]}

Pool, Vanessa L. ^{[1
]}

Parilla, Philip A. ^{[2
]}

Ginley, David S. ^{[2
]}

Van Hest, Maikel F. A. M. ^{[1
]}

Toney, Michael F. ^{[1
]}

机构：

[1] SLAC Natl Accelerator Lab, SSRL, Menlo Pk, CA 94025 USA

[2] Natl Renewable Energy Lab, Golden, CO 80401 USA

来源：

REVIEW OF SCIENTIFIC INSTRUMENTS | 2015年 / 86卷 / 01期

关键词：

CONTACTS;

D O I：

10.1063/1.4904848

中图分类号：

TH7 [仪器、仪表];

学科分类号：

0804 ; 080401 ; 081102 ;

摘要：

Rapid thermal processing (RTP) is widely used for processing a variety of materials, including electronics and photovoltaics. Presently, optimization of RTP is done primarily based on ex-situ studies. As a consequence, the precise reaction pathways and phase progression during the RTP remain unclear. More awareness of the reaction pathways would better enable process optimization and foster increased adoption of RTP, which offers numerous advantages for synthesis of a broad range of materials systems. To achieve this, we have designed and developed a RTP instrument that enables real-time collection of X-ray diffraction data with intervals as short as 100 ms, while heating with ramp rates up to 100 degrees Cs-1, and with a maximum operating temperature of 1200 degrees C. The system is portable and can be installed on a synchrotron beamline. The unique capabilities of this instrument are demonstrated with in-situ characterization of a Bi2O3-SiO2 glass frit obtained during heating with ramp rates 5 degrees Cs-1 and 100 degrees Cs-1, revealing numerous phase changes. (C) 2015 AIP Publishing LLC.

引用

页数：7

共 50 条

[41] In-situ synchrotron X-ray diffraction study of scorodite at high pressure
Fan, Dawei
Ma, Maining
Wei, Shuyi
Li, BaoSheng
Chen, Zhiqiang
Xie, Hongsen
HIGH TEMPERATURES-HIGH PRESSURES, 2013, 42 (03) : 203 - 209
[42] In-situ x-ray diffraction study of the crystallization kinetics of mesoporous titania
Kirsch, BL
Riley, AE
Richman, EK
Tolbert, SH
ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2004, 227 : U1543 - U1543
[43] In-situ X-ray diffraction study of Langmuir-Blodgett deposition
Durbin, MK
Malik, A
Richter, AG
Huang, KG
Dutta, P
LANGMUIR, 1997, 13 (24) : 6547 - 6549
[44] IN-SITU X-RAY DIFFRACTION STUDIES OF IRON ORE SINTER PHASES
Scarlett, N. V. Y.
Pownceby, M. I.
Christensen, A. N.
Madsen, I. C.
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2002, 58 : C363 - C363
[45] In-situ X-ray diffraction of corrosion products formed on iron surfaces
Takahashi, Y
Matsubara, E
Suzuki, S
Okamoto, Y
Komatsu, T
Konishi, H
Mizuki, J
Waseda, Y
MATERIALS TRANSACTIONS, 2005, 46 (03) : 637 - 642
[46] In-situ synchrotron X-ray diffraction study of scorodite at high pressure
Fan, D. (fandawei@vip.gyig.ac.cn), 2013, Old City Publishing (42)
[47] ONLINE PROCESSING OF PHARMACEUTICAL MATERIALS USING IN-SITU X-RAY-DIFFRACTION
MACCALMAN, ML
ROBERTS, KJ
KERR, C
HENDRIKSEN, B
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1995, 28 : 620 - 622
[48] Thermal expansion coefficient of carbon-supported Pt nanoparticles: In-situ X-ray diffraction study
Leontyev, I. N.
Kulbakov, A. A.
Allix, M.
Rakhmatullin, A.
Kuriganova, A. B.
Maslova, O. A.
Smirnova, N. V.
PHYSICA STATUS SOLIDI B-BASIC SOLID STATE PHYSICS, 2017, 254 (05):
[49] Thermal expansion and compressibility of alamosite (PbSiO3) determined by in-situ synchrotron X-ray diffraction
Cunha, T. R.
Sampaio, D. V.
Pena, R. B.
Moulton, B. J. A.
Lancelotti, R. F.
Alabarse, F. G.
Rodrigues, A. D.
Pizani, P. S.
CERAMICS INTERNATIONAL, 2022, 48 (23) : 34350 - 34354
[50] Thermal Stress Estimation of Tungsten Fiber Reinforced Titanium Composite by In-situ X-ray Diffraction Method
Masayuki, Nishida
Masashi, Haneoka
Tatsuya, Matsue
Tian, Jing
Takao, Hanabusa
INTERNATIONAL CONFERENCE ON RESIDUAL STRESSES 9 (ICRS 9), 2014, 768-769 : 335 - +

← 1 2 3 4 5 →