Novel N,S- and S,S-substituted dienes synthesized from mercapto triazole and some amine derivatives

被引：6
|
作者：
Ibis, Cemil [1 ]
Aydinli, Goeksin [1 ]
机构：
[1] Univ Istanbul, Fac Engn, Dept Chem, TR-34320 Istanbul, Turkey
来源：
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 2007年 / 182卷 / 07期
关键词：
mono(thio)substituted nitrodiene; 2-nitrohalodiene; 3-mercapto-1,2,4-triazole; morpholine; piperazine; N; S-substituted nitrodiene;
D O I：
10.1080/10426500701196499
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
2-Nitrodiene 1 reacted with 3-mercapto-1,2,4-triazole and cyclohexyl thiol to yield compounds 3 and4, respectively. Compounds 7a-d were obtained by reactions of 6a-d with 2. The novel N,S-substituted dienes 9a-c were obtained by treatment of compound 6b with the piperazine derivatives 8a-c. Compound 6b was reacted with 10 to give compound 11 as a new morpholine derivative. Compound 6b gave a new monobutadienyl homopiperazine 13 when reacted with homopiperazine in methylene chloride. Compound 4 was structurally characterized by single-crystal X-ray diffraction.
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收藏
页码：1427 / 1436
页数：10
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