Synthesis of Hybrid Fullerene Oxide[C60(O)n, (n≥1)] - Silver Nanoparticle Composites and Their Catalytic Activity for Reduction of 2-, 3-, 4-Nitroaniline

被引：2
|
作者：
Park, Jeong Hoon [1 ]
Ko, Jeong Won [2 ]
Ko, Weon Bae [1 ,2 ,3 ]
机构：
[1] Sahmyook Univ, Grad Sch, Dept Convergence Sci, 815 Hwarang Ro, Seoul 01795, South Korea
[2] Sahmyook Univ, Nanomat Res Inst, 815 Hwarang Ro, Seoul 01795, South Korea
[3] Sahmyook Univ, Dept Chem, 815 Hwarang Ro, Seoul 01795, South Korea
来源：
ELASTOMERS AND COMPOSITES | 2019年 / 54卷 / 03期
关键词：
Fullerene oxide[C-60(O)(n; ) (n >= 1); Silver nanoparticle; Ultrasonic irradiation; Catalytic activity; Nitroanilines; DYES;
D O I：
10.7473/EC.2019.54.3.252
中图分类号：
O63 [高分子化学（高聚物）];
学科分类号：
070305 ; 080501 ; 081704 ;
摘要：
Fullerene oxide[C-60(O)(n), (n >= 1)] was synthesized by dissolving fullerene[C-60] and 3-chloroperoxybenzoic acid in toluene under refluxing condition for 5 h. Hybrid fullerene oxide-silver nanoparticle composites were synthesized by dissolving fullerene oxide and silver nitrate[AgNO3] in diethylene glycol under ultrasonic irradiation for 3 h. The synthesized hybrid nanocomposites were characterized by X-ray diffraction, scanning electron microscopy, and ultraviolet-visible[UV-vis] spectroscopy. The catalytic activity for the reduction of various nitroanilines[NAs] was identified by UV-vis spectrophotometer. The efficiency of the catalytic reduction by the synthesized hybrid nanocomposites has an order of 4-NA > 2-NA > 3-NA.
引用
收藏
页码：252 / 256
页数：5
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