Crystal structure of 1-(4-propanoyl-2,4-dihydro-5-methyl-2-phenyl-3H-pyrazol-3-oneimine)2-aminobenzene, C19H20N4O, and of 1-(4-butanoyl-2,4-dihydro-5-methyl-2-phenyl-3H-pyrazol-3-oneimine) 2-aminobenzene, C20H22N4O

被引：0
|
作者：
Uzoukwu, BA
Gloe, K
Duddeck, H
Rademacher, O
机构：
[1] Tech Univ Dresden, Inst Anorgan Chem, D-01062 Dresden, Germany
[2] Univ Hannover, Inst Organ Chem, D-30167 Hannover, Germany
来源：
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2001年 / 216卷 / 02期
关键词：
D O I：
暂无
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
C19H20N4O, monoclinic, P12(1)/n1 (No. 14), a = 9.228(1) Angstrom, b = 9.3599(8) Angstrom, c = 19.781(3) Angstrom, beta = 100.69(2)degrees, V = 1678.9 Angstrom (3), Z = 4, R-gt(F) = 0.043, wR(ref)(F-2) = 0.123, T = 293 K. C20H22N4O, triclinic. P (1) over bar (No. 2), a = 8.830(2) Angstrom, b = 9.171(2) Angstrom, c = 11.400(3) Angstrom, alpha = 77.96(2)degrees, beta = 77.41(2)degrees, gamma = 83.97(2)degrees, V = 879.4 Angstrom (3), Z = 2, R-gt(F) = 0.042, wR(ref)(F-2) = 0.119, T = 293 K.
引用
收藏
页码：251 / 254
页数：4
相关论文
共 50 条
  • [31] Crystal structure of 2-(5-phenyl-1-(quinolin-2-yl)-4,5-dihydro-1H-pyrazol-3-yl)phenol, C24H19N3O
    Zeng, Dai
    Tan, Kai
    Fang, Ziyan
    Xing, Aiping
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2023, 238 (06): : 1153 - 1155
  • [32] 2-(4-Chlorophenyl)-4-[1-(4-chlorophenyl)-3-methyl-1H-pyrazol-5-yl]-5-methyl-1H-pyrazol-3(2H)-one
    Rabnawaz, Muhammad
    Shah, Muhammad Raza
    Ng, Seik Weng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O2569 - U535
  • [33] STRUCTURE OF BIS(4-BENZOYL-2,4-DIHYDRO-5-METHYL-2-PHENYL-3H-PYRAZOL-3-ONATO-O,O')-(DIMETHYL SULFOXIDE-O)DIOXOURANIUM(VI)
    RYAN, RR
    JARVINEN, GD
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1987, 43 : 1295 - 1298
  • [34] 1,5-Dimethyl-4-{[(3-methyl-5-oxo-1-phenyl-4,5-dihydro-1H-pyrazol-4-ylidene)(thiophen-2-yl)methyl]amino}-2-phenyl-1H-pyrazol-3(2H)-one
    Zhu, Hualing
    Ban, Litong
    Zhang, Pingping
    Zhao, Xinxin
    Ren, Junjie
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O476 - U1594
  • [35] Crystal structure of 1-(4-chlorophenyl)-4-benzoyl-3-methyl-1H-pyrazol-5-ol, C17H13ClN2O2
    Xu, Li-Ying
    Chen, Chen-chen
    Chen, Meng-Qi
    Chang, Yue
    Sang, Rui-ge
    Zhang, Heng-Qiang
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2023, 238 (05): : 959 - 961
  • [36] Crystal structure of 2-(3-chloro-phenyl)-5-methyl-4-[1-(5-methyl-4-p-tolyl- thiazol-2-ylimino)-ethyl]-2,4-dihydro-pyrazol-3-one, C23H21ClN4OS
    Thakar, Amit S.
    Friedrich, Holger B.
    Joshi, Krishnakant T.
    Maguire, Glenn E. M.
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2013, 228 (04): : 471 - 472
  • [37] 4-[(Z)-(2,4-dimethylphenylamino)phenylmethylene]-3-methyl-1-phenyl-1H-pyrazol-5(4H)-one
    Ma, Rong-Ming
    Sun, Shao-Fa
    Ng, Seik Weng
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O4679 - O4680
  • [38] EXTRACTION AND SPECTROPHOTOMETRIC DETERMINATION OF CERIUM(IV) WITH 4-BENZOYL-2,4-DIHYDRO-5-METHYL-2-PHENYL-3H-PYRAZOL-3-ONE
    ARORA, HC
    VENKATESWARLU, C
    RAO, GN
    INDIAN JOURNAL OF CHEMISTRY SECTION A-INORGANIC BIO-INORGANIC PHYSICAL THEORETICAL & ANALYTICAL CHEMISTRY, 1980, 19 (05): : 500 - 501
  • [39] Crystal structure of (4Z)-4-((4-iodoanilino)(phenyl)methyl]-3-methyl-1-phenyl-1H-pyrazol-5-(4H)-one, C23H18IN3O
    Xu, Liang
    Yang, Yan-Yun
    Wang, Bing
    Kang, Ting-Guo
    Li, Yan-Li
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2012, 227 (03): : 377 - 378
  • [40] 4-[(3,4-Dimethoxybenzylidene)amino]-5-(5-methyl-1-phenyl-1H -pyrazol-4-yl)-2,4-dihydro-3H-1,2,4-triazole-3-thione
    Nayak, Soukhyarani Gopal
    Poojary, Boja
    MOLBANK, 2019, (01)
12345