2-[1-(3-Oxo-1,3-dihydro-2-benzofuran-1-yl)-1H-benzimidazol-2-yl]benzoic acid methanol solvate

被引：0
|
作者：
Shi, Guang [1 ]
Ma, Li [1 ]
Deng, Hong [1 ]
机构：
[1] S China Nomal Univ, Sch Chem & Environm, Guangzhou 510006, Guangdong, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷
关键词：
CRYSTAL;
D O I：
10.1107/S1600536810026851
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The condensation of 2-carboxybenzaldehyde with 1,2-phenylenediamine unexpectedly yielded the title compound, C22H14N2O4 center dot CH4O. The benzimidazole ring system is almost perpendicular to the phthalazine ring system, making a dihedral angle of 88.4 (5)degrees. Intermolecular O-H...N and O-H...O hydrogen-bonding interactions stabilize the crystal structure.
引用
收藏
页码：O2034 / U1337
页数：10
相关论文
共 50 条
  • [21] 1,3-Bis(1H-benzimidazol-2-yl)-2-oxa-propane
    Chen, Ying
    Guo, Jixi
    Yun, Ruirui
    Wu, Huilu
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O948 - U1374
  • [22] N-[1-(1H-Benzimidazol-2-yl)-2-(5-chloro-3-methyl-1-phenyl-1H-pyrazol-4-yl)vinyl]benzamide
    Kaushik, Darpan
    Maan, Namita
    MOLBANK, 2011, (03)
  • [23] {2-[2-(1H-1,3-benzimidazol-2-yl)ethyliminomethyl]-4-bromophenolato} thiocyanatocopper(II) methanol solvate
    Qiu, XH
    Tong, X
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : M1470 - M1471
  • [24] 1-{2-[2-(1H-Benzimidazol-1-yl)ethoxy]ethyl}-1H-benzimidazol-3-ium hexafluorophosphate
    Sun, Sheng-Fu
    Xu, Jin
    Qin, Da-Bin
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1171 - U917
  • [25] 3-[(1H-Benzimidazol-2-yl)sulfanylmethyl]benzonitrile
    Lin, Jin Rui
    He, Jia
    Qian, Yang
    Zhao, Hong
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O1358 - U2563
  • [26] Synthesis of 4-[(1H-Benzimidazol-2-yl)sulfanyl]benzaldehyde and 2-({4-[(1H-Benzimidazol-2-yl)sulfanyl]phenyl}methylidene)hydrazine-1-carbothioamide
    Ubeid, Mustafa Turki
    Thabet, Hamdy Khamees
    Abu Shuheil, Mohamed Yousef
    MOLBANK, 2021, 2021 (03)
  • [27] 1,4-Bis(1H-benzimidazol-2-yl)benzene methanol monosolvate
    Su, Jiang-Bo
    Lin, Shen
    Chen, Li-Juan
    Yang, Ming-Xing
    Huang, Hua
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O90 - U2119
  • [28] 2,6-Bis(1H-benzimidazol-2-yl)pyridine methanol trisolvate
    Chen, Ying
    Guo, Jixi
    Huang, Xingcai
    Yun, Ruirui
    Wu, Huilu
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O1013 - U1937
  • [29] Synthesis and fluorescent properties of 2-(1H-benzimidazol-2-yl)-phenol derivatives
    Jie, OY
    Chenguang, OY
    Fujii, Y
    Nakano, Y
    Shoda, T
    Nagano, T
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 2004, 41 (03) : 359 - 365
  • [30] Bis[2-(1H-benzimidazol-2-yl)benzoato]copper(II) dihydrate
    Wang, Jun
    Dai, Chuntao
    Zhao, Dongmei
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : M1306 - U1261
12345