Preparation and characterization of polyaniline grafted silica nanoparticles
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作者:
Liu, P
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机构:
Lanzhou Univ, Coll Chem & Chem Engn, Lanzhou 730000, Peoples R ChinaLanzhou Univ, Coll Chem & Chem Engn, Lanzhou 730000, Peoples R China
Liu, P
[1
]
Liu, WM
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机构:Lanzhou Univ, Coll Chem & Chem Engn, Lanzhou 730000, Peoples R China
Liu, WM
Xue, QJ
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机构:Lanzhou Univ, Coll Chem & Chem Engn, Lanzhou 730000, Peoples R China
Xue, QJ
机构:
[1] Lanzhou Univ, Coll Chem & Chem Engn, Lanzhou 730000, Peoples R China
[2] Chinese Acad Sci, State Key Lab Solid Lubricat, Lanzhou Inst Chem Phys, Lanzhou 730000, Peoples R China
来源:
POLYMERS & POLYMER COMPOSITES
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2004年
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12卷
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08期
关键词:
D O I:
暂无
中图分类号:
TB3 [工程材料学];
学科分类号:
0805 ;
080502 ;
摘要:
Polyaniline (PANI) was grafted covalently onto the surfaces of the phenylaminopropyl silica nanoparticles (PASNs) by the in-situ chemical oxidation of aniline with ammonium peroxydisulfate (APS) using a dispersion polymerization method. A percentage of grafting (PG%) of 234.0% and a grafting efficiency (GE%) of 54.1% were achieved, calculated from the results of elemental analysis (EA). The polyaniline grafted silica nanoparticles (PANI-SNs) were also characterized by FT-IR, UV/vis, TEM, XPS and TGA. The four probe conductivities were also measured.
机构:
Kyungpook Natl Univ, Dept Chem, Grad Sch, Taegu 702701, South KoreaKyungpook Natl Univ, Dept Chem, Grad Sch, Taegu 702701, South Korea
Ragupathy, D.
Gopalan, A.
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机构:
Kyungpook Natl Univ, Dept Chem, Grad Sch, Taegu 702701, South Korea
Kyungpook Natl Univ, Dept Nanosci & Technol, Taegu 702701, South KoreaKyungpook Natl Univ, Dept Chem, Grad Sch, Taegu 702701, South Korea
Gopalan, A.
Kim, Kyeong-Wung
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机构:
Kyungpook Natl Univ, Dept Nanosci & Technol, Taegu 702701, South KoreaKyungpook Natl Univ, Dept Chem, Grad Sch, Taegu 702701, South Korea
Kim, Kyeong-Wung
Lee, Kwang Pill
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机构:
Kyungpook Natl Univ, Dept Chem, Grad Sch, Taegu 702701, South Korea
Kyungpook Natl Univ, Dept Nanosci & Technol, Taegu 702701, South KoreaKyungpook Natl Univ, Dept Chem, Grad Sch, Taegu 702701, South Korea