Preparation and characterization of polyaniline grafted silica nanoparticles

被引:0
|
作者
Liu, P [1 ]
Liu, WM
Xue, QJ
机构
[1] Lanzhou Univ, Coll Chem & Chem Engn, Lanzhou 730000, Peoples R China
[2] Chinese Acad Sci, State Key Lab Solid Lubricat, Lanzhou Inst Chem Phys, Lanzhou 730000, Peoples R China
来源
POLYMERS & POLYMER COMPOSITES | 2004年 / 12卷 / 08期
关键词
D O I
暂无
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Polyaniline (PANI) was grafted covalently onto the surfaces of the phenylaminopropyl silica nanoparticles (PASNs) by the in-situ chemical oxidation of aniline with ammonium peroxydisulfate (APS) using a dispersion polymerization method. A percentage of grafting (PG%) of 234.0% and a grafting efficiency (GE%) of 54.1% were achieved, calculated from the results of elemental analysis (EA). The polyaniline grafted silica nanoparticles (PANI-SNs) were also characterized by FT-IR, UV/vis, TEM, XPS and TGA. The four probe conductivities were also measured.
引用
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页码:695 / 698
页数:4
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