Synthesis and characterization of poly (Itaconic Acid-m-Phen-ylenediamine)

被引：0
|
作者：
Wang, Chuanxing [1 ]
Wang, Pengfei [1 ]
Xu, Qinhong [1 ]
Wei, Zhe [1 ]
Wu, Yumin [1 ]
机构：
[1] Qingdao Univ Sci & Technol, Coll Chem Engn, Qingdao 266042, Peoples R China
来源：
PROCEEDINGS OF THE 2016 INTERNATIONAL CONFERENCE ON INNOVATIVE MATERIAL SCIENCE AND TECHNOLOGY (IMST 2016) | 2016年 / 139卷
关键词：
low temperature solution polycondensation; itaconyl chloride; polymer; inherent viscosity; characterization;
D O I：
暂无
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
With Itaconyl chloride and m-phenylenediamine as raw materials, poly(itaconic acid-m-phenylenediamine) was synthesized by the low temperature solution polycondensation we reported. The effects of initial temperature and reaction time on polycondensation were investigated. And the product was characterized by H-1-NMR, FT-IR and TGA. The results showed that the polycondensation should carry out at a low temperature. The initial temperature should be lower 0 degrees C. The polycondensation time was 90-100 minutes. Under these conditions, the thermal stability was good and its inherent viscosity was about 1.4. The spectra of FT-IR and 1H-NMR confirmed its structure.
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页码：18 / 24
页数：7
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