Preparation of Amine Functionalized Porous Silica by Ultrasonic Technique for the Methylation Reaction of Phenol with Dimethyl Carbonate

被引：0

作者：

Zhang, Xuehong ^{[1
]}

Liu, Shubin ^{[1
]}

Gao, Yanlei ^{[1
]}

Zhang, Yunxiao ^{[1
]}

Ren, Lei ^{[1
]}

Hu, Ruisheng ^{[1
]}

Chen, Rufen ^{[2
]}

机构：

[1] Shijiazhuang Univ, Dept Chem, Shijiazhuang 050035, Peoples R China

[2] Hebei Normal Univ, Coll Chem & Mat, Shijiazhuang 050024, Peoples R China

来源：

JOURNAL OF THE CHEMICAL SOCIETY OF PAKISTAN | 2013年 / 35卷 / 05期

关键词：

Amine functionalized porous silica; Ultrasonic technique; Methylation reaction; O-METHYLATION; HETEROGENEOUS CATALYST; EFFICIENT; MCM-41;

D O I：

暂无

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Amine functionalized silica catalysts, including (3-aminopropyltrimethoxysilane (APTMS)) NH2/SiO2, (Diazabicycloundecene/SiO2) DBU/SiO2 and (1, 5, 7-triazabicyclo [4, 4, 0] dec-5-ene/SiO2) TBD/SiO2, which were characterized by Si-29 NMR, elemental analysis and indicator dye adsorption, were prepared by ultrasonic technique under mild conditions. Such hybrid solid bases showed high catalytic activity and well reusability towards the methylation reaction of phenol with dimethyl carbonate (DMC).

引用

页码：1284 / 1287

页数：4

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