Synthesis and Crystal Structure of 1,2,4-Triazol-5(4H)-one Derivative

被引：0
|
作者：
Ye, Dong-Ju [1 ]
Feng, Xiao-Liang [1 ]
Zhang, Zheng-Hong [1 ]
机构：
[1] Quzhou Coll, Coll Chem & Mat Engn, Quzhou 324000, Peoples R China
来源：
ASIAN JOURNAL OF CHEMISTRY | 2012年 / 24卷 / 11期
关键词：
Crystal structure; Synthesis; 1,2,4-Triazole; BIOLOGICAL-ACTIVITIES; CYCLOPROPANE MOIETY; DFT CALCULATION; DESIGN;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A new triazole compound, C17H15N3OCl2, has been synthesized and the crystal structure was determined by a single crystal X-ray diffraction study. The crystal symmetry is monoclinic, space group P2(1)/n, with a = 8.1479(17) angstrom, b = 7.9177(17) angstrom, c = 25.774(5) angstrom, alpha = 90 degrees, beta = 92.976(4)degrees, gamma = 90 degrees. An extensive three-dimensional network was observed due to the pi-pi interactions.
引用
收藏
页码：5286 / 5288
页数：3
相关论文
共 50 条
  • [41] Synthesis of 3-(tri/difluoromethyl)-1H-1,2,4-triazol-5(4H)-ones via the cyclization of hydrazinecarboxamides with tri/difluoroacetic anhydride
    You, Yi
    Chen, Yueji
    You, Chenhui
    Wang, Junwen
    Weng, Zhiqiang
    ORGANIC & BIOMOLECULAR CHEMISTRY, 2019, 17 (42) : 9343 - 9347
  • [42] 3,3′-Dimethyl-4,4′-(hexane-1,6-diyl)bis[1H-1,2,4-triazol-5(4H)-one]
    Ustabas, Resat
    Coruh, Ufuk
    Unluer, Dilek
    Hokelek, Tuncer
    Ermis, Emel
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O2615 - U957
  • [43] Crystal structure of (E)-4,4′-(diazene-1,2-diyl)bis(1-nitro-1H-1,2,4-triazol-5(4H)-one)-acetonitrile (1:1), C6H5N11O6
    Zhu, Jiaping
    Jin, Shaohua
    Yu, Yuehai
    Chen, Shusen
    Shu, Qinghai
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2016, 231 (03): : 677 - 678
  • [44] 3-(1-Adamantyl)-4-amino-1-(2-benzoyl-1-phenylethyl)-1H-1,2,4-triazol-5(4H)-thione
    Lahsasni, Siham
    Ei-Emam, Ali A.
    El-Brollosy, Nasser R.
    Quah, Ching Kheng
    Fun, Hoong-Kun
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1439 - +
  • [45] Synthesis and pancreatic lipase inhibitory activities of some 1,2,4-triazol-5(3)-one derivatives
    Ozdemir, Yusuf
    Bekircan, Olcay
    Baltas, Nimet
    Mentese, Emre
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 2020, 57 (12) : 4239 - 4253
  • [46] Crystal Structure and DFT Studies of a Triazole Derivative: 4-(2-Hydrobenzylideneamino)-3-(1,2,4-triazol-4-yl-methyl)1H-1,2,4-triazole-5(4H)-thione
    LI Wei-hua1
    2. Graduate School of the Chinese Academy of Sciences
    3. Key Laboratory of Advanced Materials
    ChemicalResearchinChineseUniversities, 2007, (03) : 343 - 348
  • [47] Crystal structure and DFT studies of a triazole derivative:: 4-(2-hydrobenzylideneamino)-3-(1,2,4-triazol-4-yl-methyl) 1H-1,2,4-triazole-5 (4H)-thione
    Li Wei-hua
    Zhang Shu-fang
    Liu Fa-qian
    Hou Bao-rong
    CHEMICAL RESEARCH IN CHINESE UNIVERSITIES, 2007, 23 (03) : 343 - 348
  • [48] 3,3′-Diisopropyl-4,4′-(hexane-1,6-diyl)bis-[1H-1,2,4-triazol-5(4H)-one] dihydrate
    Koysal, Yavuz
    Isik, Samil
    Sancak, Kemal
    Unver, Yasemin
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O3907 - O3909
  • [49] Synthesis, spectroscopic characterization, calculational studies and in vitro antitumoral activity of 4-(3-(1H-imidazol-1-yl)propyl)-(thiophen-2-ylmethyl)-1H-1,2,4-triazol-5(4H)-one
    Suleymanoglu, Nevin
    Ustabas, Resat
    Alpaslan, Yelda Bingol
    Unver, Yasemin
    Turan, Mustafa
    Sancak, Kemal
    JOURNAL OF MOLECULAR STRUCTURE, 2011, 989 (1-3) : 101 - 108
  • [50] 3-methyl-1-phenyl-4,5-dihydro-1,2,4-triazol-5(1H)-one
    Jing, Heng
    Zhu, Hong-Jun
    Liu, Shan
    Zheng, Wei
    Wu, Ya-Ming
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O4318 - O4319
12345