Influence of pressure on filtration of aqueous alumina suspensions

被引:8
|
作者
Hirata, Yoshihiro [1 ]
Fukunaga, Tomoyuki [1 ]
Matsunaga, Naoki [2 ]
Sameshima, Soichiro [1 ]
机构
[1] Kagoshima Univ, Dept Chem Biotechnol & Chem Engn, Kagoshima 8900065, Japan
[2] Miyazaki Univ, Dept Environm Robot, Miyazaki 8892192, Japan
关键词
Slip casting; Porosity; Al2O3; CERAMIC NANOPARTICLES; CONSOLIDATION; PARTICLES; BEHAVIOR; FIELD;
D O I
10.1016/j.ceramint.2012.10.180
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The dispersibility of colloidal alumina particles (median size 310 nm) was related to the surface potential, the solid concentration in a suspension and the pressure applied to the particles. The consolidation behavior of colloidal alumina particles with an isoelectric point pH 8.7 was examined using a developed pressure filtration apparatus at 1-10 MPa of applied pressure. The height of 7 or 20 vol% alumina suspensions at pH 3.0, 7.8 and 9.0 as a function of filtration time was fitted by a filtration model developed for a flocculated suspension rather than a traditional filtration model for a dispersed suspension. An increased pressure, a decrease of particle concentration and a porous microstructure of colloidal cake reduced the consolidation time of alumina suspension. The wet alumina compacts were significantly compressed during filtration but relaxed after the release of the applied pressure. However, the packing density of alumina compact after calcination at 700 degrees C was almost independent of the filtration pressure and controlled by the structure of network of alumina particles in a solution. (C) 2012 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
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页码:3547 / 3554
页数:8
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