N,N′-(2,2′-Dithiodi-o-phenylene)bis-(furan-2-carboxamide)

被引：3
|
作者：
Raftery, James [1 ]
Lallbeeharry, Hiteyeshi [2 ]
Bhowon, Minu G. [2 ]
Laulloo, Sabina J. [2 ]
Joule, John A. [1 ]
机构：
[1] Univ Manchester, Sch Chem, Manchester M13 9PL, Lancs, England
[2] Univ Mauritius, Dept Chem, Reduit, Mauritius
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷
关键词：
ANTIBACTERIAL ACTIVITY; COMPLEXES; DERIVATIVES;
D O I：
10.1107/S1600536808038828
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The reaction of 2,20-dithiobis(benzenamine) with furan-2-carbonyl chloride produced the bis-amide title compound, C22H16N2O4S2, which, in the crystal, formed a helix; the structure consists of two planar furanoylbenzenamines related by an improper rotation of 96.3 degrees about the S-S bond. The N-furanoylbenzenamine units are planar (maximum deviations = 0.316 and 0.132 angstrom). Each electron-deficient acylfuran stacks (centroid-centroid separations of the two pairs of pi-pi stacked aromatic rings are 3.918 and 3.953 angstrom) with the electron-rich benzenamine of the other N-furanoylbenzenamine unit, leading to a spiral structure. The conformation is stabilized by two bifurcated intramolecular N-H center dot center dot center dot (O,S) interactions.
引用
收藏
页码：O16 / U1407
页数：12
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