Characterization of the polymorphs of aminoacetonitrile hydrochloride and crystal structure of the stable polymorph

被引:5
|
作者
Wishkerman, Sara [1 ]
Bernstein, Joel [1 ]
机构
[1] Ben Gurion Univ Negev, Dept Chem, IL-84105 Beer Sheva, Israel
来源
CRYSTENGCOMM | 2006年 / 8卷 / 03期
关键词
D O I
10.1039/b515447b
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The three polymorphs of aminoacetonitrile hydrochloride have been reinvestigated and characterized by a variety of methods. The phase transformation from Form III to Form II to Form I was studied by thermal methods (DSC) and optical microscopy. Single-crystal X-ray diffraction studies (XRD), powder X-ray diffraction studies (PXRD) and spectroscopic studies (infrared and Raman) were carried out on for Form III.
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页码:245 / 249
页数:5
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