2,4-difluorobenzaldehyde benzoylhydrazone and 2,4-dichlorobenzaldehyde benzoylhydrazone are isostructural at 120 K with Z′=2:: complex sheets built from N-H•••O, C-H•••O and C-H•••π(arene) hydrogen bonds

被引:5
|
作者
Wardell, SMSV
Ferreira, MD
de Souza, MVN
Wardell, JL
Low, JN
Glidewell, C [1 ]
机构
[1] Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland
[2] Fiocruz MS, Far Manguinhos, Inst Tecnol Farm, BR-21041250 Rio De Janeiro, Brazil
[3] Univ Fed Rio de Janeiro, Inst Quim, Dept Quim Inorgan, BR-21945970 Rio De Janeiro, Brazil
[4] Univ Aberdeen, Dept Chem, Old Aberdeen AB24 3UE, Scotland
来源
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY | 2006年 / 62卷
关键词
D O I
10.1107/S0108270106001995
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
At 120 K, 2,4-diflorobenzaldehydebenzoylhydrazone, C14H10F2N2O, (I), and 2,4-dichlorobenzaldehyde benzoylhydrazone, C14H10Cl2N2O, (II), are isomorphous and isostructural in P2(1)/n with Z' = 2. In each structure, eight independent hydrogen bonds, viz. two of N-H center dot center dot center dot O type, five of C-H center dot center dot center dot O type and one of C-H center dot center dot center dot pi(arene) type, link the molecules into complex sheets, within which two independent one-dimensional substructures can be identified.
引用
收藏
页码:O118 / O121
页数:4
相关论文
共 50 条
  • [41] BREAKING C-H BONDS WITH COBALT AND O-2
    REINAUD, OM
    THEOPOLD, KH
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1994, 207 : 481 - INOR
  • [42] H2O2-driven enzymatic oxyfunctionalization of tertiary C-H bonds
    Huang, Yawen
    Li, Huanhuan
    Zhang, Pengpeng
    Zhang, Yalan
    Duan, Peigao
    Zhang, Wuyuan
    CHEMICAL COMMUNICATIONS, 2023, 59 (60) : 9219 - 9222
  • [43] Synthesis and characterization of two new chiral Kemp's acid derivatives: structures fixed by a peculiar system of N-H•••O, C-H•••O and C-H•••N hydrogen bonds
    Pazout, Richard
    Maixner, Jaroslav
    Pechacek, Jan
    Vilhanova, Beata
    Kacer, Petr
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-CRYSTALLINE MATERIALS, 2016, 231 (09): : 531 - 539
  • [44] Microwave spectroscopic and theoretical studies on the phenylacetylene•••H2O complex: C-H•••O and O-H•••π hydrogen bonds as equal partners
    Goswami, Mausumi
    Arunan, E.
    PHYSICAL CHEMISTRY CHEMICAL PHYSICS, 2011, 13 (31) : 14153 - 14162
  • [45] O-H...O-N and H2C-H...O hydrogen bonds
    Hernandez, E.
    Mas, M.
    Molins, E.
    Rovira, C.
    Veciana, J.
    Angewandte Chemie (International Edition in English), 1993, 32 (06):
  • [46] 2-Nitrophenoxyacetanilide:: a chain of rings generated by C-H•••O hydrogen bonds
    Glidewell, C
    Low, JN
    Skakle, JMS
    Wardell, JL
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2004, 60 (04): : O290 - O292
  • [47] Influence of N-H•••O and C-H•••O hydrogen bonds on the 17O NMR tensors in crystalline uracil:: Computational study
    Ida, R
    De Clerk, M
    Wu, G
    JOURNAL OF PHYSICAL CHEMISTRY A, 2006, 110 (03): : 1065 - 1071
  • [48] Can C-H•••F-C hydrogen bonds alter crystal packing features in the presence of N-H•••O=C hydrogen bond?
    Yadav, Hare Ram
    Choudhury, Angshuman Roy
    JOURNAL OF MOLECULAR STRUCTURE, 2017, 1150 : 469 - 480
  • [49] E versus Z isomers of Fischer aminocarbene complex [Mo(CO)4(PPh3){C(NHCy)(2-furyl)}]: N-H•••O versus C-H•••O intramolecular hydrogen bonds
    Landman, Marile
    Conradie, Jeanet
    JOURNAL OF MOLECULAR STRUCTURE, 2015, 1094 : 36 - 45
  • [50] N-H•••N hydrogen bonding in the four independent molecules of (2S,4S,5R)(-)-2-(1H-imidazol-2-yl)-3,4-dimethyl-5-phenyl-1,3-oxazolidine, with C-H•••πarene, C-H•••O and C-H•••πC=C interactions
    Gallagher, JF
    Briody, JM
    Cantwell, BP
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1998, 54 : 1331 - 1335