Synthesis and characterization of single-crystalline vanadium pentoxide by the low-temperature of glycothermal method

被引：11
|
作者：
Chiang, Tzu Hsuan [1 ]
Chen, Tso-Ming [1 ]
机构：
[1] Natl United Univ, Dept Energy Engn, Nan Shi Li 36003, Miaoli, Taiwan
来源：
MATERIALS LETTERS | 2015年 / 157卷
关键词：
Ceramics; Structural; Powder technology; Glycothermal; ELECTROCHEMICAL CHARACTERIZATION; HYDROTHERMAL SYNTHESIS; V2O5;
D O I：
10.1016/j.matlet.2015.05.112
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Single-crystalline vanadium pentoxide (V2O5) powder was prepared by a low-temperature of glycothermal method in which ammonium metavanadate (NH4VO3) solution was mixed with ethylene glycol, heated at 100 degrees C for 1 h, and annealed at 300 degrees C for 1 h. X-ray diffraction (XRD) and transmission electron microscopy (TEM) characterizations were coordinated with orthorhombic V2O5. The smallest rice-shaped V2O5 particles, with sizes of 2-3 mu m, were obtained when the powders were annealed at 400 degrees C for 1 h. The low temperature of the glycothermal method used in preparing orthorhombic V2O5 was simpler to use than other methods. (C) 2015 Elsevier B.V. All rights reserved.
引用
收藏
页码：205 / 208
页数：4
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