Dangerous Tendency in the Presentation of GC-MS Identification Results

被引:2
|
作者
Zenkevich, I. G. [1 ]
机构
[1] St Petersburg State Univ, Dept Chem, St Petersburg 198504, Russia
关键词
gas chromatography-mass spectrometry; multicomponent mixtures; unacceptable identification results; CHEMICAL-COMPOSITION; ESSENTIAL OILS;
D O I
10.1134/S1061934813130108
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A dangerous tendency in the presentation of the results of the GC-MS identification of complex mixture components is discussed. This is an increasing number of publications where unacceptable results are presented. The main signs of them are the absence of a correspondence between the lists of identified compounds and the general principles of chromatographic retention, the indication of erroneous retention indices and chemical names, the unreliable chemical origin of analytes, etc. The main criteria for revealing such errors are the control of the chromatographic elution order of analytes and the absolute values of their retention indices.
引用
收藏
页码:1158 / 1161
页数:4
相关论文
共 50 条
  • [21] Identification and determination of (+)-sesamin in Semen Cuscutae by capillary GC and GC-MS
    Li, Y
    Ye, M
    Liu, HW
    Ji, XH
    Yan, YN
    CHINESE CHEMICAL LETTERS, 2000, 11 (12) : 1073 - 1076
  • [22] Effects of sampling methodologies on GC-MS and GC-olfactometry results
    Goodner, KL
    Mahattanatawee, K
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2005, 230 : U5 - U6
  • [23] GC-MS IDENTIFICATION OF PROTHIOPHOS IN IMPORTED PRESERVED CABBAGE
    PETZINGER, G
    BARRY, TL
    STENSON, M
    BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY, 1983, 31 (01) : 116 - 119
  • [24] Identification and Analysis of the Impurities for Triethylboron by GC-MS Method
    Su, Pengfei
    Xiu-tian-feng, E.
    Wang, Jingna
    Zhu, Yanlong
    Zhang, Gao
    Chang, Hai
    Liu, Ke
    Meng, Zihui
    PROPELLANTS EXPLOSIVES PYROTECHNICS, 2022, 47 (04)
  • [25] IDENTIFICATION OF COMPONENTS OF LAURENCIAE SPECIES BY GC-MS AND FDMS
    CACCAMESE, S
    RINEHART, KL
    SHAW, PD
    JOHNSON, RD
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1975, 170 (AUG24): : 19 - 19
  • [26] HPTLC and GC-MS for separation and identification of eugenol in plants
    Rusu, Mihai Lucian
    Marutoiu, Constantin
    Sandu, Ion
    Tita, Dumitru
    Gogoasa, Ioan
    Barbu, Constantin-Horia
    Popescu, Andreea
    JPC-JOURNAL OF PLANAR CHROMATOGRAPHY-MODERN TLC, 2007, 20 (02) : 139 - 140
  • [27] Identification of natural indigo in historical textiles by GC-MS
    Degani, Laura
    Riedo, Chiara
    Chiantore, Oscar
    ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2015, 407 (06) : 1695 - 1704
  • [28] GC-MS IDENTIFICATION OF ACTIVE METABOLITE OF OXACILLIN IN MAN
    MURAI, Y
    NAKAGAWA, T
    UNO, T
    CHEMICAL & PHARMACEUTICAL BULLETIN, 1980, 28 (01) : 362 - 364
  • [29] HPTLC and GC-MS for Separation and Identification of Eugenol in Plants
    Mihai Lucian Rusu
    Constantin Marutoiu
    Ion Sandu
    Dumitru Tita
    Ioan Gogoasa
    Constantin-Horia Barbu
    Andreea Popescu
    JPC – Journal of Planar Chromatography – Modern TLC, 2007, 20 : 139 - 140
  • [30] Identification of photodegradation products of nilvadipine using GC-MS
    Mielcarek, J
    Stobiecki, M
    Franski, R
    JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 2000, 24 (01) : 71 - 79