Synthesis of core-shell (nano)particles involving TiO2, SiO2, Al2O3 and polylactide

被引：2
|
作者：
Bernard, Alexandre [1 ]
Chisholm, Malcolm H. [1 ]
机构：
[1] Newman & Wolfrom Lab, Columbus, OH 43210 USA
来源：
POLYHEDRON | 2012年 / 46卷 / 01期
关键词：
Polylactide; Nanoparticles; Coating; Surface; NANOPARTICLES; STARCH; POLYMERIZATION; ACID;
D O I：
10.1016/j.poly.2012.07.017
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The synthesis of core-shell particles of TiO2, SiO2 and basic Al2O3 are described based on surface modification of the particles and a solution reaction involving L-lactide and a catalyst such as tin octanoate or 4-dimethylaminopyridine. Surface modification involves treating the particles with titanium isopropoxide, lactic acid or glycolic acid. A similar approach taken with sand, Fe3O4, Co3O4, BaTiO3. montmorillonite clay or starch yielded varying results. Polymer coatings were characterized by Fourier-transform infrared spectrometry, solid-state C-13 NMR and mass balance. (C) 2012 Elsevier Ltd. All rights reserved.
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页码：1 / 7
页数：7
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