Growth and Structure of Sr3Yb2(BO3)4 Crystal

被引：0
|
作者：
Lin Fu-Lin [1 ,2 ]
Huang Jian-Hua [1 ]
Gong Xing-Hong [1 ]
Huang Xiao-Ying [1 ]
Lin Yan-Fu [1 ]
Chen Yu-Jin [1 ]
Huang Yi-Dong [1 ]
机构：
[1] Chinese Acad Sci, Fujian Inst Res Struct Matter, Key Lab Optoelect Mat Chem & Phys, Fuzhou 350002, Peoples R China
[2] Chinese Acad Sci, Grad Univ, Beijing 100039, Peoples R China
来源：
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY | 2013年 / 32卷 / 03期
基金：
中国国家自然科学基金;
关键词：
Sr3YP2(BO3)(4); Czochralski method; crystal structure; LASER OPERATION;
D O I：
暂无
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A Sr3Yb2(BO3)(4)ingle crystal was obtained by the Czochralski method. The structure of Sr3Yb2(BO3)(4)ystal was determined by single-crystal X-ray diffraction. The compound crystallizes in orthorhombic, space group Pnma with a = 7.3750(8), b = 15.9265(14), c = 8.6776(9) angstrom, V= 1019.25(18) angstrom(3), M-r= 844.18, Z= 4, D-c 5.501 g/cm(3), lambda(MoK alpha) = 0.71073 angstrom,mu = 33.835 mm(-1) F(000) = 1480, the final R= 0.0339 and wR= 0.0907 for 1090 observed reflections with I> 2 sigma(I). The structure features a three-dimensional framework composed of isolated BO3 planar triangles bridged by YbO(8)and SrO8 polyhedra. The Sr2+ and Yb3+ occupy statistically three independent sites with a C, and two Ci local symmetries.
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收藏
页码：434 / 438
页数：5
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