Reaction of (chloromethyl)trichlorosilane with 2,2-dimethylpropane-1,3-diol

被引：1
|
作者：
Lazareva, N. F. [1 ]
Sterkhova, I. V. [1 ]
机构：
[1] Russian Acad Sci, AE Favorsky Irkutsk Inst Chem, Siberian Branch, 1 Ul Favorskogo, Irkutsk 664033, Russia
来源：
RUSSIAN CHEMICAL BULLETIN | 2017年 / 66卷 / 12期
关键词：
(chloromethyl) trichlorosilane; 2,2-dimethylpropane-1,3-diol; cyclization; 2,8-dichloro-2,8-bis(chloromethyl)-5,5,11,11-tetramethyl-1,3,7,9-tetraoxa-2,8-disilacyclododecane; CHEMISTRY;
D O I：
10.1007/s11172-017-2026-y
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
(Chloromethyl)trichlorosilane reacts with 2,2-dimethylpropane-1,3-diol to produce alpha-carbofunctional heterocycles, 2-chloro-2-(chloromethyl)-5,5-dimethyl-1,3,2-dioxasilinane and 2,8-dichloro-2,8-bis(chloromethyl)-5,5,11,11-tetramethyl-1,3,7,9-tetraoxa-2,8-disilacyclododecane. The synthesized macroheterocycle is the first structurally characterized 1,3,7,9-tetraoxa-2,8-disilacyclododecane derivative.
引用
收藏
页码：2339 / 2342
页数：4
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