Reaction of (chloromethyl)trichlorosilane with 2,2-dimethylpropane-1,3-diol

被引：1

作者：

Lazareva, N. F. ^{[1
]}

Sterkhova, I. V. ^{[1
]}

机构：

[1] Russian Acad Sci, AE Favorsky Irkutsk Inst Chem, Siberian Branch, 1 Ul Favorskogo, Irkutsk 664033, Russia

来源：

RUSSIAN CHEMICAL BULLETIN | 2017年 / 66卷 / 12期

关键词：

(chloromethyl) trichlorosilane; 2,2-dimethylpropane-1,3-diol; cyclization; 2,8-dichloro-2,8-bis(chloromethyl)-5,5,11,11-tetramethyl-1,3,7,9-tetraoxa-2,8-disilacyclododecane; CHEMISTRY;

D O I：

10.1007/s11172-017-2026-y

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

(Chloromethyl)trichlorosilane reacts with 2,2-dimethylpropane-1,3-diol to produce alpha-carbofunctional heterocycles, 2-chloro-2-(chloromethyl)-5,5-dimethyl-1,3,2-dioxasilinane and 2,8-dichloro-2,8-bis(chloromethyl)-5,5,11,11-tetramethyl-1,3,7,9-tetraoxa-2,8-disilacyclododecane. The synthesized macroheterocycle is the first structurally characterized 1,3,7,9-tetraoxa-2,8-disilacyclododecane derivative.

引用

页码：2339 / 2342

页数：4

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