Determination and Analysis of Ustiloxins A and B by LC-ESI-MS and HPLC in False Smut Balls of Rice

被引：45
|
作者：
Shan, Tijiang [1 ]
Sun, Weibo [1 ]
Liu, Hao [1 ]
Gao, Shan [1 ]
Lu, Shiqiong [1 ]
Wang, Mingan [1 ]
Sun, Wenxian [1 ]
Chen, Zhiyi [2 ]
Wang, Shu [3 ]
Zhou, Ligang [1 ]
机构：
[1] China Agr Univ, Coll Agron & Biotechnol, Beijing 100193, Peoples R China
[2] Jiangsu Acad Agr Sci, Inst Plant Protect, Nanjing 210014, Jiangsu, Peoples R China
[3] Liaoning Acad Agr Sci, Inst Plant Protect, Shenyang 110161, Peoples R China
来源：
INTERNATIONAL JOURNAL OF MOLECULAR SCIENCES | 2012年 / 13卷 / 09期
关键词：
Villosiclava virens; ustiloxins A and B; false smut balls of rice; determination and analysis; LC-ESI-MS; HPLC; QUANTITATIVE ANALYTICAL PROCEDURES; ANTIMITOTIC CYCLIC-PEPTIDES; USTILAGINOIDEA-VIRENS; NATURAL-PRODUCTS; SFSTP PROPOSAL; HARMONIZATION; STRATEGIES; VALIDATION;
D O I：
10.3390/ijms130911275
中图分类号：
Q5 [生物化学]; Q7 [分子生物学];
学科分类号：
071010 ; 081704 ;
摘要：
Ustiloxins are cyclopeptide mycotoxins produced by the pathogenic fungus Villosiclava virens of rice false smut. Ustiloxins A and B as two main mycotoxins were determined conveniently by LC-ESI-MS in the water extract from rice false smut balls which were mostly composed of the chlamydospores and mycelia of the pathogen. Both ustiloxins A and B in the water extract were also quantitatively analyzed by HPLC. This is the first report on the determination and analysis of ustiloxins A and B simultaneously by LC-ESI-MS and HPLC in false smut balls of rice.
引用
收藏
页码：11275 / 11287
页数：13
相关论文
共 50 条
  • [41] Gradient Elution LC-ESI-MS Determination of Tramadol in Rat Plasma
    Lin, Chongliang
    Ma, Jianshe
    Lin, Guanyang
    Zhou, Ziye
    Hu, Lufeng
    Wang, Xianqin
    LATIN AMERICAN JOURNAL OF PHARMACY, 2011, 30 (08): : 1500 - 1505
  • [42] Simultaneous determination of paracetamol and caffeine in human plasma by LC-ESI-MS
    Wang, Anna
    Sun, Jin
    Feng, Haijun
    Gao, Shuo
    He, Zhonggui
    CHROMATOGRAPHIA, 2008, 67 (3-4) : 281 - 285
  • [43] LC-ESI-MS Determination of Quassinoids Isobrucein B and Neosergeolide in Picrolemma sprucei Stem Infusions
    Pohlit, Adrian M.
    Jabor, Valquiria A. P.
    Amorim, Rodrigo C. das N.
    Costa e Silva, Ellen C.
    Lopes, Norberto P.
    JOURNAL OF THE BRAZILIAN CHEMICAL SOCIETY, 2009, 20 (06) : 1065 - 1070
  • [44] Rapid determination of rifaximin on dried blood spots by LC-ESI-MS
    Rao, R. Nageswara
    Vali, R. Mastan
    Ramachandra, Bondigalla
    Maurya, Pawan K.
    BIOMEDICAL CHROMATOGRAPHY, 2011, 25 (11) : 1201 - 1207
  • [45] Simultaneous determination of tramadol and acetaminophen in human plasma by LC-ESI-MS
    Zhu, Tian
    Ding, Li
    Guo, Xiaofeng
    Yang, Lin
    Wen, Aidong
    CHROMATOGRAPHIA, 2007, 66 (3-4) : 171 - 178
  • [46] Determination of Ramosetron in Rat Plasma by LC-ESI-MS and its Application
    Wang, Qing
    Pang, Lingxia
    Wang, Youpei
    Zheng, Meiqin
    Chen, XiaoLe
    Lin, Guanyang
    LATIN AMERICAN JOURNAL OF PHARMACY, 2011, 30 (10): : 2076 - 2080
  • [47] Sensitive LC-ESI-MS method for determination of tiopronin in human plasma
    Lai, L.
    Ma, L.
    Chen, X. J.
    Wang, G. J.
    Wang, J. P.
    Davey, A. K.
    CHROMATOGRAPHIA, 2006, 64 (11-12) : 655 - 659
  • [48] Identification of ustiloxins in false smut balls of rice based on high performance liquid chromatography-high resolution mass spectrometry
    Bian Yingfang
    Yu Shasha
    Mou Renxiang
    Cao Zhaoyun
    Sun Weihua
    Yang Huan
    Lin Xiaoyan
    Chen Mingxue
    CHINESE JOURNAL OF CHROMATOGRAPHY, 2015, 33 (10) : 1046 - 1050
  • [49] LC-ESI-MS analysis of iridoid glucosides in Lamium species
    Alipieva, Kahna
    Kokubun, Tetsuo
    Taskova, Rilka
    Evstatieva, Ljuba
    Handjieva, Nedjalka
    BIOCHEMICAL SYSTEMATICS AND ECOLOGY, 2007, 35 (01) : 17 - 22
  • [50] LC-ESI-MS for rapid and sensitive determination of aripiprazole in human plasma
    Zuo, Xiao-cong
    Wang, Feng
    Xu, Ping
    Zhu, Rong-hua
    Li, Huan-de
    CHROMATOGRAPHIA, 2006, 64 (7-8) : 387 - 391
12345