Determination and Analysis of Ustiloxins A and B by LC-ESI-MS and HPLC in False Smut Balls of Rice

被引：45

作者：

Shan, Tijiang ^{[1
]}

Sun, Weibo ^{[1
]}

Liu, Hao ^{[1
]}

Gao, Shan ^{[1
]}

Lu, Shiqiong ^{[1
]}

Wang, Mingan ^{[1
]}

Sun, Wenxian ^{[1
]}

Chen, Zhiyi ^{[2
]}

Wang, Shu ^{[3
]}

Zhou, Ligang ^{[1
]}

机构：

[1] China Agr Univ, Coll Agron & Biotechnol, Beijing 100193, Peoples R China

[2] Jiangsu Acad Agr Sci, Inst Plant Protect, Nanjing 210014, Jiangsu, Peoples R China

[3] Liaoning Acad Agr Sci, Inst Plant Protect, Shenyang 110161, Peoples R China

来源：

INTERNATIONAL JOURNAL OF MOLECULAR SCIENCES | 2012年 / 13卷 / 09期

关键词：

Villosiclava virens; ustiloxins A and B; false smut balls of rice; determination and analysis; LC-ESI-MS; HPLC; QUANTITATIVE ANALYTICAL PROCEDURES; ANTIMITOTIC CYCLIC-PEPTIDES; USTILAGINOIDEA-VIRENS; NATURAL-PRODUCTS; SFSTP PROPOSAL; HARMONIZATION; STRATEGIES; VALIDATION;

D O I：

10.3390/ijms130911275

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

Ustiloxins are cyclopeptide mycotoxins produced by the pathogenic fungus Villosiclava virens of rice false smut. Ustiloxins A and B as two main mycotoxins were determined conveniently by LC-ESI-MS in the water extract from rice false smut balls which were mostly composed of the chlamydospores and mycelia of the pathogen. Both ustiloxins A and B in the water extract were also quantitatively analyzed by HPLC. This is the first report on the determination and analysis of ustiloxins A and B simultaneously by LC-ESI-MS and HPLC in false smut balls of rice.

引用

页码：11275 / 11287

页数：13

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