Microwave-hydrothermal/solvothermal synthesis of kesterite, an emerging photovoltaic material

被引：19
|
作者：
Yan, Xinlong [1 ]
Michael, Elizabeth [2 ]
Komarneni, Sridhar [3 ]
Brownson, Jeffrey R. [4 ]
Yan, Zi-Feng [1 ]
机构：
[1] China Univ Petr, CNPC Key Lab Catalysis, State Key Lab Heavy Oil Proc, Qingdao 266555, Peoples R China
[2] Penn State Univ, Dept Mat Sci & Engn, University Pk, PA 16802 USA
[3] Penn State Univ, Mat Res Inst, Mat Res Lab, University Pk, PA 16802 USA
[4] Penn State Univ, Dept Energy & Mineral Engn, University Pk, PA 16802 USA
来源：
CERAMICS INTERNATIONAL | 2014年 / 40卷 / 01期
关键词：
Kesterite; Microwave-hydrothermal; Microwave-solvothermal; Band gap; HYDROTHERMAL SYNTHESIS; CU2ZNSNS4; NANOCRYSTALS;
D O I：
10.1016/j.ceramint.2013.07.108
中图分类号：
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号：
0805 ; 080502 ;
摘要：
Rapid synthesis of kesterite (Cu2ZnSnS4), an emerging photovoltaic material was achieved by microwave-hydrothermal/solvothermal (M-HIS) process. Conventional-hydrothermal (C-H) process was also used for comparison with M-H/S process. The synthesized kesterite samples were characterized by powder X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and electron diffraction and UV vis spectroscopy. Nanophase kesterite, which is potentially suitable for coating was synthesized in ethylene glycol. Band gap values were calculated from UV vis spectra of several synthetic kesterites and these values are close to the reported values for kesterite. (C) 2013 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
引用
收藏
页码：1985 / 1992
页数：8
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