Synthesis of 4-(2,2-dibromovinyl)phenol and its one-pot esterification

被引：1
|
作者：
Zhang, Wensheng [1 ]
Xu, Wenjing [1 ]
Zhang, Fei [2 ]
Li, Jitao [1 ]
Liu, Mei [1 ]
Li, Wei [1 ]
机构：
[1] Jiaozuo Teachers Coll, Sch Biol & Chem Engn, Jiaozuo 450001, Peoples R China
[2] Jiaozuo Vocat Educ Ctr, Jiaozuo 450001, Peoples R China
来源：
RESEARCH ON CHEMICAL INTERMEDIATES | 2012年 / 38卷 / 3-5期
关键词：
gem-Dibromoalkene; Corey-Fuchs condition; One-pot; Synthesis; Esterification; SUZUKI-MIYAURA; 1,1-DIBROMOALKENES; ALKYNES; FACILE;
D O I：
10.1007/s11164-011-0432-6
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
In situ treatment of 4-(2,2-dibromovinyl)phenol, which was prepared from 4-hydroxybenzaldehyde and carbon tetrabromide in CH2Cl2 under Corey-Fuchs conditions, with a diverse range of acids in the presence of dicyclohexyl-carbodiimide (DCC) and 4-dimethylaminopyridine (DMAP) gave the corresponding esters in high yields.
引用
收藏
页码：957 / 964
页数：8
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