Results obtained on microwave irradiation method to prepare Ruthenium (Ru) nanoparticles on nitrogen doped carbon nanotubes (N-CNTs) are reported. The N-CNTs were prepared by chemical vapour deposition. X-ray diffraction, high resolution transmission electron microscopy (HR-TEM) and Raman techniques were used to characterise the Ru/CNT material. The results show that the microwave assisted method allows synthesis to be achieved using shorter reaction times, reduced energy consumption than conventional heating. The results of HR-TEM show a good dispersion of metals on the N-CNTs. Ru nanoparticles with very narrow size distribution and small particle size with an average diameter of 2.5 nm on N-CNTs were obtained.
机构:Jawaharlal Nehru Ctr Adv Sci Res, Int Ctr Mat Sci, Chem & Phys Mat Unit, New Chem Unit, Bangalore 560064, Karnataka, India
Panchakarla, L. S.
Govindaraj, A.
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机构:Jawaharlal Nehru Ctr Adv Sci Res, Int Ctr Mat Sci, Chem & Phys Mat Unit, New Chem Unit, Bangalore 560064, Karnataka, India
Govindaraj, A.
Rao, C. N. R.
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Jawaharlal Nehru Ctr Adv Sci Res, Int Ctr Mat Sci, Chem & Phys Mat Unit, New Chem Unit, Bangalore 560064, Karnataka, IndiaJawaharlal Nehru Ctr Adv Sci Res, Int Ctr Mat Sci, Chem & Phys Mat Unit, New Chem Unit, Bangalore 560064, Karnataka, India
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DST/CSIR Nanotech, Innovation Centre, National Centre for Nano-Structured Materials, Council for Scientific and Industrial Research, Pretoria
DST/NRF Centre of Excellence in Strong Materials and Molecular Sciences Institute, School of Chemistry, University of the Witwatersrand, JohannesburgDST/CSIR Nanotech, Innovation Centre, National Centre for Nano-Structured Materials, Council for Scientific and Industrial Research, Pretoria
Mabena L.F.
Sinha Ray S.
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DST/CSIR Nanotech, Innovation Centre, National Centre for Nano-Structured Materials, Council for Scientific and Industrial Research, Pretoria
Department of Chemical Technology, University of Johannesburg, Doornfontein, JohannesburgDST/CSIR Nanotech, Innovation Centre, National Centre for Nano-Structured Materials, Council for Scientific and Industrial Research, Pretoria
Sinha Ray S.
Mhlanga S.D.
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DST/NRF Centre of Excellence in Strong Materials and Molecular Sciences Institute, School of Chemistry, University of the Witwatersrand, JohannesburgDST/CSIR Nanotech, Innovation Centre, National Centre for Nano-Structured Materials, Council for Scientific and Industrial Research, Pretoria
Mhlanga S.D.
Coville N.J.
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DST/NRF Centre of Excellence in Strong Materials and Molecular Sciences Institute, School of Chemistry, University of the Witwatersrand, JohannesburgDST/CSIR Nanotech, Innovation Centre, National Centre for Nano-Structured Materials, Council for Scientific and Industrial Research, Pretoria