Study of deformation mechanisms in flash-sintered yttria-stabilized zirconia by in-situ micromechanical testing at elevated temperatures

被引:29
|
作者
Cho, Jaehun [1 ]
Li, Jin [1 ]
Wang, Han [1 ]
Li, Qiang [1 ]
Fan, Zhe [2 ]
Mukherjee, A. K. [3 ]
Rheinheimer, W. [1 ]
Wang, Haiyan [1 ,4 ]
Zhang, X. [1 ]
机构
[1] Purdue Univ, Sch Mat Engn, W Lafayette, IN 47907 USA
[2] Oak Ridge Natl Lab, Oak Ridge, TN USA
[3] Univ Calif Davis, Dept Chem Engn & Mat Sci, Davis, CA 95616 USA
[4] Purdue Univ, Sch Elect & Comp Engn, W Lafayette, IN 47907 USA
来源
MATERIALS RESEARCH LETTERS | 2019年 / 7卷 / 05期
关键词
Flash sintering; deformation mechanism; in-situ microcompression test; dislocation; VACANCY FORMATION ENERGIES; REDUCING GRAIN-BOUNDARY; SHAPE-MEMORY; SOLUTE SEGREGATION; DISLOCATION-MOTION; ACTIVATION-ENERGY; CREEP; DIFFUSION; BEHAVIOR; MICROSTRUCTURE;
D O I
10.1080/21663831.2019.1575924
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Flash sintering has received wide attention lately due to its ultrafast densification process at low sintering temperature. However, the deformability of flash-sintered ceramics remains poorly understood. Yttria-stabilized zirconia (YSZ) was processed by flash sintering to study deformation mechanism. Transmission electron microscopy studies show that the flash-sintered YSZ contains ultrafine grains and dislocations. Strain rate jump tests at elevated temperature by in-situ microcompression indicate the existence of a large threshold stress. The activation energy of deformation is approximate to 145kJ/mol, similar to the activation energy for oxygen vacancy migration. The deformation mechanisms of the flash-sintered YSZ at elevated temperatures are discussed. [GRAPHICS] . IMPACT STATEMENTThe current study reveals the underlying deformation mechanisms of flash-sintered 3YSZ that shows considerable plasticity over the temperature range of 450-650 degrees C via in-situ microcompression test.
引用
收藏
页码:194 / 202
页数:9
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