Effect of Ultrasonic Treatment on the Solubility of Sodium Sulphate Using Response Surface Methodology

被引:1
|
作者
Li, Hui [1 ,2 ]
Zeng, Guisheng [1 ,2 ]
Tu, Xinman [1 ,2 ]
机构
[1] Nanchang Hangkong Univ, Key Lab Jiangxi Prov Persistant Pollutants Contro, Nanchang 330063, Peoples R China
[2] Nanchang Hangkong Univ, Sch Environm & Chem Engn, Nanchang 330063, Peoples R China
基金
中国国家自然科学基金; 国家高技术研究发展计划(863计划);
关键词
Sodium sulphate; Crystallization; Ultrasonic wave; Response surface methodology; Solubility; OPTIMIZATION; CRYSTALLIZATION; EXTRACTION;
D O I
10.14233/ajchem.2013.14331
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The effect of ultrasonic treatment on the solubility of sodium sulphate was investigated in this study. The influence of several single-factor experiments including temperature, ultrasonic time, ultrasonic power and rotation rate on the solubility of sodium sulphate was carried out. Response surface methodology (RSM), based on a three level, three variable central composite design (BBD), was employed to obtain the best possible combination of temperature (X-1), ultrasonic time (X-2) and ultrasonic power (X-3) for maximum solubility according to the results from single-factor experiment. The 3-D response surface plot and the contour plot was derived from the mathematical models. The results also showed that the best conditions to attain the maximum solubility are met when temperature was 35 degrees C, time was 20 min, power was 140 w. Under this condition, the experimental yield was 52.6321 g, which was well matched with the predictive yield.
引用
收藏
页码:6222 / 6226
页数:5
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