Determination of Unsaponifiable Constituents of Deodorizer Distillates by GC-MS

被引：16

作者：

Naz, Saba ^{[1
]}

Sherazi, S. T. H. ^{[1
]}

Talpur, Farah N. ^{[1
]}

Talpur, M. Younis ^{[1
]}

Kara, Huseyin ^{[2
]}

机构：

[1] Univ Sindh, Natl Ctr Excellence Analyt Chem, Jamshoro, Pakistan

[2] Selcuk Univ, Fen Edebiyat Fak, Kimya Bolumu, TR-42075 Konya, Turkey

来源：

JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY | 2012年 / 89卷 / 06期

关键词：

Deodorizer distillate; Bioactive components; GC-MS; VEGETABLE-OILS; LIQUID-CHROMATOGRAPHY; GAS; RECOVERY;

D O I：

10.1007/s11746-011-2000-z

中图分类号：

O69 [应用化学];

学科分类号：

081704 ;

摘要：

Deodorizer distillate is an important by-product obtained during deodorization in the edible oil industries. It is a complex mixture of many health beneficial constituents like phytosterols, tocopherols and squalene. In the present study a simple gas chromatographic method with mass spectrometry was used for the separation, detection and quantification of different components present in the deodorizer distillate in a very short analysis time of 18 min. A simple saponification procedure without derivatization was used for their analysis followed by GC-MS analysis. Phytosterols concentration (21.27-25.53%) was the most abundant in canola and palm distillate samples whereas, squalene and tocopherol were present in concentration ranges of 2.89-13.21% and 1.29-5.81%, respectively. The present study revealed that the unsaponifiable fraction of deodorizer distillate could be used in cosmetic preparations due to its appreciable amount of bioactive constituents.

引用

页码：973 / 977

页数：5

共 50 条

[21] Determination of steroid hormones in blood by GC-MS/MS
Hansen, Martin
Jacobsen, Naja W.
Nielsen, Frederik K.
Bjorklund, Erland
Styrishave, Bjarne
Halling-Sorensen, Bent
ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2011, 400 (10) : 3409 - 3417
[22] Determination of Polybrominated diphenyl ethers by GC-MS/MS
Grabic, R
Crhová, S
Sebestová, M
Pacáková, V
CHEMICKE LISTY, 2002, 96 (10): : 809 - 812
[23] GC-MS/MS method for age determination of fingerprints
Szaboova, Zofia
Galbava, Paulina
Szabo, Alexandra Hengerics
Cigan, Marek
Niznansky, L'ubos
Kubinec, Robert
Blasko, Jaroslav
MONATSHEFTE FUR CHEMIE, 2017, 148 (09): : 1673 - 1678
[24] GC OR GC-MS
PRATZEL, B
STURINO, E
POLLUTION ENGINEERING, 1983, 15 (08) : 28 - 29
[25] Lipid constituents from Artemisia nilagirica: A GC-MS investigation
Khan, RA
Gupta, AK
Singh, AK
Agrawal, PK
INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 1997, 36 (05): : 453 - 455
[26] GC-MS ANALYSIS OF BIOACTIVE CONSTITUENTS OF GLOCHIDION ELLIPTICUM WT
Jayashree, Indhiramuthu
Geetha, D. H.
Rajeswari, M.
INTERNATIONAL JOURNAL OF PHARMACEUTICAL SCIENCES AND RESEARCH, 2015, 6 (06): : 2546 - 2550
[27] GC-MS analysis of bioactive constituents of indigofera suffruticosa leaves
Vijisaral Elezabeth, D.
Arumugam, S.
Journal of Chemical and Pharmaceutical Research, 2014, 6 (08) : 294 - 300
[28] GC-MS Study of Nonpolar Constituents from Scutellaria comosa
Karimov, A. M.
Drenin, A. A.
Vasina, N. A.
Botirov, E. Kh.
CHEMISTRY OF NATURAL COMPOUNDS, 2015, 51 (06) : 1188 - 1190
[29] GC-MS Study of Nonpolar Constituents of Juniperus communis Needles
G. A. Usmanova
S. V. Nekhoroshev
M. G. Kul’kov
A. V. Nekhorosheva
E. X. Botirov
Chemistry of Natural Compounds, 2018, 54 : 781 - 783
[30] Extraction and GC-MS Analysis of the Volatile Constituents of A Tractylodes macrocephala
Lin, Yin
Wang, Guang-Hua
Yuan, Ke
ASIAN JOURNAL OF CHEMISTRY, 2011, 23 (02) : 551 - 555

← 1 2 3 4 5 →