Confirmation of the structure of tetra-O-(tert-butyldimethylsilyl)-D-glucono-1,4-lactone formed by silylation of D-glucono-1,5-lactone

被引：3

作者：

Singh, J ^{[1
]}

DiMarco, J

Kissick, TP

Deshpande, P

Gougoutas, JZ

机构：

[1] Bristol Myers Squibb Co, Pharmaceut Res Inst, Mat Sci, Princeton, NJ 08543 USA

[2] Bristol Myers Squibb Co, Pharmaceut Res Inst, Proc Res & Dev, Princeton, NJ 08543 USA

来源：

CARBOHYDRATE RESEARCH | 2002年 / 337卷 / 06期

关键词：

silylation; D-glucono-1,5-lactone; D-glucono-1,4-lactone; X-ray diffraction;

D O I：

10.1016/S0008-6215(02)00014-9

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

The structure of tetra-O-(tert-butyldimethylSilyl)-D-glucono-1,4-lactone made by the silylation of D-glucono-1,5-lactone has been confirmed by single-crystal X-ray analysis. (C) 2002 Elsevier Science Ltd. All rights reserved.

引用

页码：563 / 564

页数：2

共 46 条

[41] X-ray diffraction and high-resolution NMR spectroscopic analysis of 2,4,7,8-tetra-O-acetyl-3-deoxy-α-D-manno-2-octulopyranosono-1,5-lactone
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CARBOHYDRATE RESEARCH, 2001, 330 (01) : 145 - 147
[42] 3,3':5,6-Di-O-isopropylidene-3-C-hydroxy-methyl-D-allono-1,4-lactone:: an organic structure containing large unoccupied voids
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ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O799 - O801
[43] FORMATION OF METHYL (2,7-ANHYDRO-3-DEOXY-ALPHA-D-MANNO-2-OCTULOFURANOS)ONATE UPON METHANOLYSIS OF 2,4,7,8-TETRA-O-ACETYL-3-DEOXY-ALPHA-D-MANNO-2-OCTULOPYRANOSONO-1,5-LACTONE
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[44] CRYSTAL AND MOLECULAR-STRUCTURE OF 2-ACETAMIDO-2,3-DIDEOXY-5,6-O-ISOPROPYLIDENE-D-THREO-HEX-2-ENONO-1,4-LACTONE, C11H15NO5
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ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE CRYSTAL ENGINEERING AND MATERIALS, 1978, 34 (APR) : 1226 - 1230
[45] CRYSTAL AND MOLECULAR-STRUCTURE OF (+)-6,7-8,9-10,11-TRI-O-ISOPROPYLIDENE-2,3-DIDEOXY-D-ARABINO-L-ALLO-UNDEC-2-ENONO-1,4-LACTONE, C20H30O9
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[46] SYNTHESIS OF (2R,3S,4R)-3,4-DIHYDROXYPROLINE FROM D-RIBONOLACTONE - AN APPROACH TO THE SYNTHESIS OF POLYFUNCTIONALIZED D-AMINO ACIDS FROM SUGAR LACTONES - X-RAY MOLECULAR-STRUCTURES OF 2-AZIDO-3,4-O-(R)-BENZYLIDENE-2-DEOXY-D-RIBONO-1,5-LACTONE, 2-AZIDO-2-DEOXY-D-RIBONO-1,4-LACTONE, AND (2R,3S,3R)-3,4-DIHYDROXYPROLINET
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