Preparation of Mo-Cu composite powder with high homogeneity by solution combustion synthesis

被引:10
|
作者
Chen, Zheng [1 ,2 ]
Kang, Wentao [1 ]
Li, Bingxue [1 ]
Zhang, Qiao [1 ,2 ,3 ]
Hu, Xudong [1 ]
Ding, Yi [4 ]
Liang, Shuhua [1 ,2 ]
机构
[1] Xian Univ Technol, Sch Mat Sci & Engn, Shaanxi Prov Key Lab Elect Mat & Infiltrat Technol, Xian 710048, Peoples R China
[2] Xian Univ Technol, Engn Res Ctr Conducting Mat & Composite Technol, Minist Educ, Xian 710048, Peoples R China
[3] Pinggao Grp Co Ltd, Pingdingshan 467000, Peoples R China
[4] State Grid Smart Grid Res Inst Co Ltd, State Key Lab Adv Power Transmiss Technol, Beijing 102209, Peoples R China
来源
JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&T | 2023年 / 24卷
基金
中国博士后科学基金; 中国国家自然科学基金;
关键词
Mo-Cu composite; Solution combustion synthesis; Liquid phase sintering; Composite powder; MECHANICAL-PROPERTIES; HYDROGEN REDUCTION; MICROSTRUCTURE; FABRICATION; COPPER; ROUTE;
D O I
10.1016/j.jmrt.2023.03.043
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
In order to reduce the sintering temperature of the Mo-Cu composites, solution combustion synthesis was used to fabricate ultrafine Mo-Cu composite powders, in which Mo and Cu mixed uniformly. Firstly, solution combustion synthesis was conducted to prepared mo-lybdenum and copper oxides composite powders. However, the residual carbon in the as -synthesized precursors requires additional calcination in nitrogen atmosphere during the reduction process to obtain pure Mo-Cu composite powders. Then the Mo-Cu composites were fabricated by liquid phase sintering at low temperatures of 1050-1180 degrees C using the Mo-Cu composite powders. The Mo-20Cu and Mo-30Cu composites can reach a relative density of >95% after sintering at a low temperature of 1100 degrees C, which may be attributed to both the small particle size of Mo and the high uniformity of Mo and Cu distribution.(c) 2023 The Author(s). Published by Elsevier B.V. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
引用
收藏
页码:715 / 723
页数:9
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