Acidic Nano Zeolite Clinoptillolite; Green and Heterogeneous Catalyst for One-Pot Multi-Component Synthesis of 3-Substituted-Amino Coumarins

被引:4
|
作者
Rabiei, Khadijeh [1 ]
Niyazi, Shabnam [1 ]
机构
[1] Qom Univ Technol, Fac Sci, Dept Organ Chem, Qom 37195, Iran
关键词
Novel nanocatalyst; NCP@SiO(3)PrHMTASO(3)H; aminocoumarin; green synthesis; HIGHLY EFFICIENT; AQUEOUS-SOLUTION; SULFAMIC ACID; CLINOPTILOLITE; REMOVAL; NANOPARTICLES; ADSORPTION;
D O I
10.1080/10406638.2022.2072909
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
In this study, a novel acidic natural surface-modified nanoclinoptilolite (NCP@SiO(3)PrHMTASO(3)H) have been designed, synthesized, and fully characterized using various analytical techniques (Fourier Transform Infrared Spectroscopy (FT-IR), X-ray Diffraction (XRD), Scanning Electron Microscopy (SEM), Energy-Dispersive X-ray Spectroscopy (EDS), Transmission Electron Microscopy (TEM), and Thermogravimetric-Analyses (TG). In addition, NCP@SiO(3)PrHMTASO(3)H nanocatalyst have been found to catalyze effectively the multi-component synthesis of Manich base containing coumarin moiety under solvent-free condition. This novel heterogeneous catalyst is easily recycled and reused several times.
引用
收藏
页码:3473 / 3488
页数:16
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