YbPO4 crystals in as-drawn silica-based optical fibers

被引：6
|
作者：
Lu, Zhuorui [1 ,2 ]
Vakula, Natalia [3 ]
Ude, Michele [1 ]
Cabie, Martiane [4 ]
Neisius, Thomas [4 ]
Orange, Francois [5 ]
Pigeonneau, Franck [2 ]
Petit, Laeticia [3 ]
Blanc, Wilfried [1 ]
机构：
[1] Univ Cote dAzur, Inst Phys Nice, CNRS UMR7010, Nice, France
[2] PSL Res Univ, CEMEF Ctr Mat Forming, MINES Paris, CNRS UMR 7635, CS 10207,Rue Claude Daunesse, F-06904 Sophia Antipolis, France
[3] Tampere Univ, Photon Lab, Korkeakoulunkatu 3, Tampere 33720, Finland
[4] Aix Marseille Univ, CNRS, Cent Marseille, FSCM,CP2M, F-13397 Marseille, France
[5] Univ Cote dAzur, CCMA, Nice, France
来源：
OPTICAL MATERIALS | 2023年 / 138卷
关键词：
Chemical vapor deposition; Scanning electron microscopy; Transmission electron microscopy; Silica; Fiber; CONVECTIVE HEAT-TRANSFER; THERMAL-CONDUCTIVITY; ETHYLENE-GLYCOL; FRICTION FACTOR; VIBRATIONAL-SPECTRA; WATER-NANOFLUID; GLASS; NANOPARTICLES; VISCOSITY; FE3O4;
D O I：
10.1016/j.optmat.2023.113644
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
MCVD germanosilica glass embedded with YbPO4 crystals were for the first time drawn into optical fibers. So-lution doping was used to embed the crystals in the silica soot prior to the collapsing step. We demonstrate, using scanning/transmission electron microscopes and confocal Raman microscope, that YbPO4 crystals survive not only the MCVD process but also the drawing process despite the high temperature involved (up to 2100 degrees C) during fabrication processes. The fiber contains 100 nm-crystals with the same composition and structure as the as-prepared crystals. During the drawing process, these crystals tend to have a preferential orientation of their c -axis along the drawing direction. These results open a new route to fabricate glass-based composite fibers containing crystalline particles without additional post heat-treatment.
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页数：6
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