Synthesis of Substituted Cyclohexenones by Reaction of Chalcones with Acetoacetic Acid Amides

被引：0
|
作者：
Nosova, N. V. [1 ]
Sokolov, A. A. [1 ]
Gein, V. L. [1 ]
Dmitriev, M. V. [2 ]
Mokrushin, I. G. [2 ]
机构：
[1] Perm State Pharmaceut Acad, Perm 614990, Russia
[2] Perm State Natl Res Univ, Perm 614990, Russia
来源：
RUSSIAN JOURNAL OF GENERAL CHEMISTRY | 2023年 / 93卷 / 11期
关键词：
cyclohexenones; acetoacetic acid amides; benzalacetophenone; 4-methoxybenzalacetophenone;
D O I：
10.1134/S1070363223110026
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
New 4-aryl-2-oxo-6-phenyl-3-cyclohexene-1-carboxamides were obtained by the reaction of N-substituted acetoacetic acid amides with benzalacetophenone and 4-methoxybenzalacetophenone in alcohol in the presence of potassium hydroxide. Structure of the prepared compounds was proved using IR, H-1 and C-13 NMR spectroscopy, mass spectrometry and X-ray analysis data.
引用
收藏
页码：2742 / 2748
页数：7
相关论文
共 50 条
  • [21] Synthesis and characterization of α-substituted chalcones and alkenones
    McClure, Emily
    Dolph, Linnea
    Sieck, Stephen
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2018, 255
  • [22] Synthesis of 4,5-trans-substituted cyclohexenones
    Kuendig, E. Peter
    Sau, Manisankar
    Perez-Luna, Alejandro
    SYNLETT, 2006, (13) : 2114 - 2118
  • [23] DIETHYL PHOSPHITE REACTION WITH ACETOACETIC ACID ESTER
    PUDOVIK, AN
    ZIMIN, MG
    SOBANOV, AA
    ZHURNAL OBSHCHEI KHIMII, 1970, 40 (04): : 936 - &
  • [24] Synthesis of new functionally substituted 2-oxo(thioxo)nicotinic acid amides and nitriles by SNVin reaction
    Dyachenko, V. D.
    Bityukova, O. S.
    Dyachenko, A. D.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2011, 47 (09) : 1335 - 1340
  • [25] Silica sulfuric acid: a reusable solid catalyst for the synthesis of N-substituted amides via the Ritter reaction
    Rapolu, Rajesh Kumar
    NabaMukul, Buragohain
    Bommineni, Srinath Reddy
    Potham, Rajender
    Mulakayala, Naveen
    Oruganti, Srinivas
    RSC ADVANCES, 2013, 3 (16) : 5332 - 5337
  • [26] Synthesis of new functionally substituted 2-oxo(thioxo)nicotinic acid amides and nitriles by SNVin reaction
    V. D. Dyachenko
    O. S. Bityukova
    A. D. Dyachenko
    Russian Journal of Organic Chemistry, 2011, 47 : 1335 - 1340
  • [27] SYNTHESIS OF SUBSTITUTED AROMATIC AMIDES
    SHARMA, S
    KAUR, A
    BHATIA, MS
    JOURNAL OF THE INDIAN CHEMICAL SOCIETY, 1989, 66 (11) : 829 - 831
  • [28] REACTION OF SUBSTITUTED LITHIUM AMIDES WITH DIBORANE
    SCHWARTZ, LD
    KELLER, PC
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1972, 94 (09) : 3015 - &
  • [29] REACTION OF SUBSTITUTED LITHIUM AMIDES WITH DIBORANE
    SCHWARTZ, LD
    KELLER, PC
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1971, (MAR-A): : 78 - &
  • [30] SYNTHESIS AND IR SPECTRA OF N-SUBSTITUTED DICARBOXYLIC ACID AMIDES
    AUGUSTIN, M
    KOHLER, M
    HARZER, R
    ZEITSCHRIFT FUR CHEMIE, 1971, 11 (08): : 311 - &
12345