A simple and convenient electrochenical detection cell for capillary electrophoresis is described in this paper. In this cell, alignment of the capillary working electrode with the separation capillary outlet can be achieved precisely and easily without the aid of the ndcropositioner or ndcroscope. With end-column detection, the applicability of the cell as an amperometric detector for capillary electrophoresis is demonstrated by running several phenolic compounds in 50 μm i.d. capillary with a capillary Pt electrode as the working electrode. Results obtained are satisfactory.
Min Sheng ZHANG (Department of Chemistry. Sun Yat-sen University of Medical Sciences. Guangzhou 510089 College of Chemistry and Chemical Engineering. Zhongshan University.
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Min Sheng ZHANG (Department of Chemistry. Sun Yat-sen University of Medical Sciences. Guangzhou 510089 College of Chemistry and Chemical Engineering. Zhongshan University.