Determination of arylamine compounds in waste water using solid-phase extraction and reversed-phase high performance liquid chromatography

被引：0

作者：

Zhao, Shu-Li ^{[1
]}

Wei, Fu-Sheng ^{[1
]}

Zou, Han-Fa ^{[2
]}

Xu, Xiao-Bai ^{[3
]}

机构：

[1] China Natl. Environ. Monitoring Ctr., Beisihuan Dong Lu, Beijing, 100029, China

[2] Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian, 116012, China

[3] Res. Ctr. for Eco-Environ. Sciences, Chinese Academy of Sciences, Beijing, 100085, China

来源：

Journal of Liquid Chromatography and Related Technologies | 1998年 / 21卷 / 05期

关键词：

High performance liquid chromatography - Methanol - Separation - Solvent extraction - Ultraviolet detectors - Wastewater treatment;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

A simple, rapid, and sensitive method for determining 10 arylamine compounds in wastewater sample using solid-phase extraction (SPE) and high performance liquid chromatography (HPLC) with UV detection is developed. An SPE procedure is described for extracting and preconcentrating the arylamines on Sep-Pak C18 cartridges with methanol as solvent. A mobile phase gradient of acetonitrile-water was used for the separation and determination of the arylamines. The detection limits of the compounds were in the range of 0.1-1.5 μg/L. Recoveries were 84-107% for 10 arylamines at concentration levels of 20 μg/L with relative standard deviations of less than 8% (n = 4).

引用

页码：717 / 724

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