Gas chromatography and gas chromatography/mass spectrometry for the characterization of complex mixtures of large oligosaccharides

被引:0
|
作者
Karlsson, H. [1 ]
Hansson, G.C. [1 ]
机构
[1] Univ of Gothenburg, Sweden
关键词
Chromatographic Analysis--Gas;
D O I
暂无
中图分类号
学科分类号
摘要
High temperature gas chromatography and gas chromatography/mass spectrometry are used in the characterization of complex natural mixtures of permethylated oligosaccharides released from proteins or lipids. The high resolution allows separation of isomeric compounds and the mass range extends to oligosaccharides around molecular mass 2000 daltons or 10 sugar residues for isomalto-oligosaccharides. The mass spectra of permethylated oligosaccharide alditols from mucin glycopeptides are very informative and the approach allows a simple and rapid characterization of these complex components.
引用
收藏
页码:820 / 824
相关论文
共 50 条
  • [41] Characterization of cyclitol glycosides by gas chromatography coupled to mass spectrometry
    Ruiz-Aceituno, L.
    Carrero-Carralero, C.
    Ruiz-Matute, A. I.
    Ramos, L.
    Sanz, M. L.
    Martinez-Castro, I.
    JOURNAL OF CHROMATOGRAPHY A, 2017, 1484 : 58 - 64
  • [42] Characterization of archaeological frankincense by gas chromatography-mass spectrometry
    Mathe, C
    Culioli, G
    Archier, P
    Vieillescazes, C
    JOURNAL OF CHROMATOGRAPHY A, 2004, 1023 (02) : 277 - 285
  • [43] DERIVATIVES FOR CHARACTERIZATION OF PHOSPHOSERINE AND PHOSPHOTHREONINE BY GAS CHROMATOGRAPHY MASS SPECTROMETRY
    SHIEH, JJ
    DESIDERIO, DM
    ANALYTICAL LETTERS, 1977, 10 (11) : 831 - 834
  • [44] Characterization of acetals by means of capillary gas chromatography mass spectrometry
    DelaRuelle, H
    Klok, J
    Rinken, M
    Felix, M
    RAPID COMMUNICATIONS IN MASS SPECTROMETRY, 1995, 9 (15) : 1507 - 1511
  • [45] Characterization of Dialkyl Phosphites by Gas Chromatography-Mass Spectrometry
    Zenkevich, I. G.
    Nosova, V. E.
    JOURNAL OF ANALYTICAL CHEMISTRY, 2018, 73 (12) : 1162 - 1176
  • [46] CHARACTERIZATION OF LAURENCIA SPECIES BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY
    CACCAMESE, S
    HAGER, LP
    RINEHART, KL
    SETZER, RB
    BOTANICA MARINA, 1979, 22 (01) : 41 - 46
  • [47] Features of the Identification of Trialkyl Phosphites in Reaction Mixtures and Their Characterization by Gas Chromatography-Mass Spectrometry
    Zenkevich, I. G.
    Nosova, V. E.
    JOURNAL OF ANALYTICAL CHEMISTRY, 2019, 74 (13) : 1305 - 1319
  • [48] Characterization of complex hydrocarbons in cigarette smoke condensate by gas chromatography-mass spectrometry and comprehensive two-dimensional gas chromatography-time-of-flight mass spectrometry
    Lu, X
    Zhao, MY
    Kong, HW
    Cai, JL
    Wu, JF
    Wu, M
    Hua, RX
    Liu, JF
    Xu, GW
    JOURNAL OF CHROMATOGRAPHY A, 2004, 1043 (02) : 265 - 273
  • [49] CHARACTERIZATION OF NATURAL BITUMENS BY PYROLYSIS-GAS CHROMATOGRAPHY AND PYROLYSIS-GAS CHROMATOGRAPHY MASS-SPECTROMETRY
    PHILP, RP
    RUBLE, T
    GALVEZSINIBALDI, A
    CZECHOWSKI, F
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1990, 200 : 46 - GEOC
  • [50] CHARACTERIZATION OF AZAARENES IN IXTOC-I OIL BY GAS-CHROMATOGRAPHY AND GAS CHROMATOGRAPHY-MASS SPECTROMETRY
    DELEON, IR
    MCCARTHY, LV
    RASCHKE, CK
    OVERTON, EB
    LASETER, JL
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1980, 180 (AUG): : 11 - ENVR