Technological parameters in the synthesis of 1,1,1-trichloroethane from vinylidene chloride

被引：0

作者：

Milchert, Eugeniusz ^{[1
]}

Goc, Waldemar ^{[1
]}

Stefanska, Jolanta ^{[1
]}

Pazdzioch, Waldemar ^{[1
]}

机构：

[1] Technical Univ of Szczecin, Szczecin, Poland

来源：

Industrial and Engineering Chemistry Research | 1996年 / 35卷 / 10期

关键词：

Catalysts - Chemical reactions - Composition - Ethane - Hydrogen inorganic compounds - Modification - Raw materials - Solvents - Temperature - Thermodynamic properties - Vinyl resins;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

The optimum parameters in the synthesis of 1,1,1-trichloroethane during the reaction between vinylidene chloride and hydrogen chloride are as follows: temperature, 22°C; catalyst (FeCl3) concentration, 0.3% by weight;, equimolar ratio of raw materials; VDC flow rate, 0.22-0.23 cm3 cm-3 h-1. Changing these parameters does not result in considerable change in the product yield.

引用

页码：3290 / 3294

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