REGENERATIVE HIGH-RESOLUTION NMR SPECTROSCOPY.

被引:0
|
作者
Konstantinov, Yu.S.
Smirnov, A.M.
机构
来源
关键词
D O I
暂无
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
A description is given of a high-resolution NMR spectrometer in which the signal sensor is a sideband spin generator working in multiple-frequency mode. A method is considered for adjusting and monitoring the phase shift in the feedback circuit of this generator with an error of 10** minus **3 rad, which provides for measuring spectral intervals in excess of 10 Hz with an error not more than 10** minus **4 Hz for NMR linewidths of 0. 2 Hz. A method is also given for suppressing the parasitic modulation that occurs when there is inhomogeneous broadening of the NMR line of the working specimen. The spectrometer also allows one to measure the longitudinal-relaxation time T//1.
引用
收藏
页码:447 / 450
相关论文
共 50 条
  • [41] HIGH-RESOLUTION NMR SPECTROSCOPY OF GLIOBLASTOMA-INITIATING CELLS
    Ramm, Paul
    Vollmann-Zwerenz, Arabel
    Beier, Christoph
    Aigner, Ludwig
    Bogdahn, Ulrich
    Kalbitzer, Hans R.
    Hau, Peter
    NEURO-ONCOLOGY, 2010, 12 : 123 - 123
  • [42] High-Resolution 1H NMR Spectroscopy of Solids
    Hodgkinson, Paul
    ANNUAL REPORTS ON NMR SPECTROSCOPY, VOL 72, 2010, 72 : 185 - 223
  • [43] A subband ARMA modeling approach to high-resolution NMR spectroscopy
    Tomczak, M
    Djermoune, EH
    JOURNAL OF MAGNETIC RESONANCE, 2002, 158 (1-2) : 86 - 98
  • [44] In situ observation of protein phosphorylation by high-resolution NMR spectroscopy
    Philipp Selenko
    Dominique P Frueh
    Simon J Elsaesser
    Wilhelm Haas
    Steven P Gygi
    Gerhard Wagner
    Nature Structural & Molecular Biology, 2008, 15 : 321 - 329
  • [45] Removal of a time barrier for high-resolution multidimensional NMR spectroscopy
    Jaravine, Victor
    Ibraghimov, Ilgis
    Orekhov, Vladislav Yu
    NATURE METHODS, 2006, 3 (08) : 605 - 607
  • [46] Simple high-resolution NMR spectroscopy as a tool in molecular biology
    Mureddu, Luca
    Vuister, Geerten W.
    FEBS JOURNAL, 2019, 286 (11) : 2035 - 2042
  • [47] Microcoil high-resolution magic angle spinning NMR spectroscopy
    Janssen, Hans
    Brinkmann, Andreas
    Van, Eck, Ernst R. H.
    Van, Bentum, P. Jan M.
    Kentgens, Arno P. M.
    Journal of the American Chemical Society, 2006, 128 (27): : 8722 - 8723
  • [48] Quantification of lignin–carbohydrate linkages with high-resolution NMR spectroscopy
    Mikhail Balakshin
    Ewellyn Capanema
    Hanna Gracz
    Hou-min Chang
    Hasan Jameel
    Planta, 2011, 233 : 1097 - 1110
  • [49] A Study of Water–Protein Interactions by High-Resolution NMR Spectroscopy
    V. P. Kutyshenko
    Molecular Biology, 2001, 35 : 80 - 88
  • [50] HIGH-RESOLUTION SOLID-STATE NMR-SPECTROSCOPY
    REINHOLD, M
    AMERICAN LABORATORY, 1982, 14 (02) : 164 - &