Rapid screening of oleuropein from olive leaves using matrix solid-phase dispersion and high-performance liquid chromatography

被引：0
|
作者：
机构：
[1] Rashidipour, Marzieh
[2] Heydari, Rouhollah
[3] Feizbakhsh, Alireza
[4] Hashemi, Payman
来源：
Heydari, R. (rouhollahheydari@yahoo.com) | 1600年 / AOAC International卷 / 97期
关键词：
Matrix solid-phase dispersion (MSPD) methodology as a quick and easy extraction method has been developed to extract oleuropein from Olea europaea leaves. This method has been compared with conventional maceration and Soxhlet extraction (SOXE) methods. Variables affecting MSPD; such as the sorbent material; the ratio of sample to sorbent material; elution solvent; and volume of the elution solvent; have been fully evaluated and optimized. Oleuropein was successfully extracted by silica sorbent with 350 μL of dichloromethane- methanol (70 + 30; v/v) as the elution solvent. The calibration curve showed good linearity (r2 = 0.9985) and precision (RSD;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
Journal article (JA)
引用
收藏
相关论文
共 50 条
  • [41] Determination of noscapine in human plasma using solid-phase extraction and high-performance liquid chromatography
    Chollet, DF
    Ruols, C
    Arnera, V
    JOURNAL OF CHROMATOGRAPHY B, 1997, 701 (01): : 81 - 85
  • [42] DETERMINATION OF GLICLAZIDE IN SERUM BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY USING SOLID-PHASE EXTRACTION
    NOGUCHI, H
    TOMITA, N
    NARUTO, S
    NAKANO, S
    JOURNAL OF CHROMATOGRAPHY-BIOMEDICAL APPLICATIONS, 1992, 583 (02): : 266 - 269
  • [43] Determination of atazanavir in human plasma using solid-phase extraction and high-performance liquid chromatography
    Cateau, E
    Tournier, N
    Dupuis, A
    Le Moal, G
    Venisse, N
    JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 2005, 39 (3-4) : 791 - 795
  • [44] ANALYSIS OF MILRINONE IN PLASMA USING SOLID-PHASE EXTRACTION AND HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY
    ODDIE, CJ
    JACKMAN, GP
    BOBIK, A
    JOURNAL OF CHROMATOGRAPHY, 1986, 374 (01): : 209 - 214
  • [45] Determination of Norfloxacin and Enrofloxacin by Solid-Phase Microextraction/High-Performance Liquid Chromatography
    Kumar, Ashwini
    Dhingra, Gaurav
    Malik, Ashok Kumar
    Tewary, Dhananjay K.
    JOURNAL OF AOAC INTERNATIONAL, 2008, 91 (06) : 1339 - 1343
  • [46] Determination of Estazolam in Plasma by High-Performance Liquid Chromatography with Solid-Phase Extraction
    Masatomo Miura
    Tadashi Ohkubo
    Kazunobu Sugawara
    Naoyuki Okuyama
    Koichi Otani
    Analytical Sciences, 2002, 18 : 525 - 528
  • [47] Analysis of imazaquin in soybeans by solid-phase extraction and high-performance liquid chromatography
    Guo, C.
    Hu, J. -Y.
    Chen, X. -Y.
    Li, J. -Z.
    BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY, 2008, 80 (02) : 173 - 177
  • [48] Determination of Polysorbates in foods by solid-phase extraction and high-performance liquid chromatography
    Nomura, Chie
    Kitagawa, Mikiya
    Yoshida, Masaharu
    Tanaka, Yukio
    JOURNAL OF THE FOOD HYGIENIC SOCIETY OF JAPAN, 2007, 48 (03): : 64 - 68
  • [49] Determination of Furfural in Beer by High-Performance Liquid Chromatography with Solid-Phase Extraction
    Li, Mei
    Yang, Zhaoxia
    Yang, Mei
    Shan, Lianju
    Dong, Jianjun
    JOURNAL OF THE INSTITUTE OF BREWING, 2009, 115 (03) : 226 - 231
  • [50] SOLID-PHASE DERIVATIZATION OF THIOLS - APPLICATION TO HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY
    MILLOT, MC
    SEBILLE, B
    MAHIEU, JP
    JOURNAL OF CHROMATOGRAPHY, 1986, 354 : 155 - 167
12345