[1] Max-Planck-Institut für Eisenforschung GmbH, Max-Planck-Str. 1, Düsseldorf,40237, Germany
[2] Department of Materials, The University of Manchester, Manchester,UK,M13 9PL, United Kingdom
[3] Henry Royce Institute for Advanced Materials, The University of Manchester, Manchester,UK,M13 9PL, United Kingdom
[4] Department of Earth and Environmental Sciences, The University of Manchester, Manchester,UK,M13 9PL, United Kingdom