Synthesis characterization and application of butyl acrylate mediated eco-friendly silver nanoparticles using ultrasonic radiation

被引:0
|
作者
Saxena, Indu [1 ]
Ejaz, Syed Mohammad [1 ]
Gupta, Aditya [1 ]
机构
[1] Univ Lucknow, Dept Chem, Lucknow 226007, India
关键词
Silver nanoparticles; Ultra-sonication; Powder X-ray diffraction; Transmission electron microscopy; Dye degradation; GREEN SYNTHESIS; LEAF EXTRACT; BIOSYNTHESIS; CARRAGEENAN; DEGRADATION;
D O I
10.1016/j.heliyon.2024.e28309
中图分类号
O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];
学科分类号
07 ; 0710 ; 09 ;
摘要
In the present investigation, with an effort to provide appropriate material for future applications, we have touched on two viable advancement targets: the production of silver nanoparticles (Ag-NPs) employing an ultrasonic approach and the use of Ag-NPs in environmental remediation. A green economical method was involved to prepare Ag-NPs using butyl acrylate as a stabilizer. The following techniques were used for analysing Ag-NPs: energy dispersive X-ray spectroscopy (EDX), transmission electron microscopy (TEM), field emission scanning electron microscopy (FESEM), powder X-ray diffraction (XRD), and Fourier transformed infrared (FT-IR) spectroscopy. X-ray diffraction (XRD) analysis for the lattice characteristics showed that Ag-NPs have a face-centered structure with an average crystallite size of 9.51-11.83 nm. FE-SEM and TEM analysis were used for morphological investigations, and revealed that Ag-NPs had a spherical shape with an average particle size of 16.27 nm. The EDX profile displayed a strong signal at similar to 3.0 keV, which indicated that the samples comprised silver. UV-Visible spectrophotometer with the absorption maximum occurring between 401 and 411 nm further confirmed the formation of AgNPs. The dye degradation effect of synthesized Ag-NPs on methylene blue and Rhodamine B was analyzed to assess their ability for environmental remediation, and results showed that around 100% of the dye degradation effect. This study has provided a most plausible mechanism for the dye degradation.
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页数:11
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