Single-Step Pressureless Synthesis of the High-Purity Ti 3 AlC 2 MAX-Phase by Fast Heating

被引：1

作者：

Kirian, I. M. ^{[1
]}

Lakhnik, A. M. ^{[1
]}

Khyzhun, O. Yu ^{[2
]}

V. Zagorulko, I. ^{[1
]}

Nikolenko, A. S. ^{[3
]}

Rud, O. D. ^{[1
]}

机构：

[1] NAS Ukraine, GV Kurdyumov Inst Met Phys, 36 Academician Vernadsky Blvd, UA-03142 Kiev, Ukraine

[2] NAS Ukraine, IM Frantsevych Inst Problems Mat Sci, 3 Omeljan Pritsak Str, UA-03142 Kiev, Ukraine

[3] NAS Ukraine, VE Lashkaryov Inst Semicond Phys, 41 Nauky Ave, UA-03028 Kiev, Ukraine

来源：

METALLOPHYSICS AND ADVANCED TECHNOLOGIES | 2023年 / 45卷 / 10期

关键词：

MAX phase; pressureless synthesis; fast heating; ball milling; ELASTIC PROPERTIES;

D O I：

10.15407/mfint.45.10.1165

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

A simple approach is presented to synthesise the high-purity MAX phase by the pressureless method. This method is featured by the short time in duration. The process is executed with a high heating rate (up to congruent to 10 2 K/min) that inhibits the formation of the objectionable phases and limits elemental loss due to the short-time process. The samples containing congruent to 96% wt. of the MAX phase Ti 3 AlC 2 are successfully synthesised using the proposed technique.

引用

页码：1165 / 1177

页数：107

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