LONG-CHAIN FATTY-ACIDS ESTERIFIED BY ACTION OF ALKYL CHLOROFORMATES AND ANALYZED BY CAPILLARY GAS-CHROMATOGRAPHY

被引：11
|
作者：
HUSEK, P
机构：
[1] Institute of Endocrinology, 116 94 Prague 1
来源：
JOURNAL OF CHROMATOGRAPHY-BIOMEDICAL APPLICATIONS | 1993年 / 615卷 / 02期
关键词：
D O I：
10.1016/0378-4347(93)80349-9
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
Long-chain fatty acids can be instantaneously converted into methyl, ethyl or chloroethyl esters by the action of corresponding alkyl chloroformates. The reaction is catalysed by pyridine and proceeds in acetonitrile in the presence of a small amount of the corresponding alcohol. The reproducibility is high and the yield exceeds 95%.
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页码：334 / 338
页数：5
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