BULBED CAPILLARY EXTERNAL REFERENCING METHOD USING A SUPERCONDUCTING MAGNET NMR INSTRUMENT

被引:43
|
作者
MOMOKI, K [1 ]
FUKAZAWA, Y [1 ]
机构
[1] IND RES INST,KANAZAWA KU,YOKOHAMA 236,JAPAN
关键词
BULBED CAPILLARY METHOD; SUPERCONDUCTING MAGNET NMR INSTRUMENT; BULBED CAPILLARY 1H SHIFTS; BULBED CAPILLARY 13C SHIFTS;
D O I
10.2116/analsci.10.53
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Whether the bulbed capillary external referencing method developed with an electromagnet NMR instrument can be performed also with a superconducting magnet instrument by only changing g(cy) from 2pi/3 to 0 is studied. As the result, the same bulbed capillary and procedures giving high precisions and accuracies are found to be applicable to either electromagnet or superconducting magnet instrument and to either H-1 or even C-13 spectra. Thus, the validity of the generalized bulbed capillary theories and the superiorities of the bulbed capillary method over previous referencing methods are made clear.
引用
收藏
页码:53 / 58
页数:6
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