(2S,4R)-2-[(1R)-1-(4-Bromophenyl)-2-nitroethyl]-4-ethylcyclohexanone

被引：1

作者：

Zhang, Chi-Xiao ^{[1
]}

Zhang, Yan-Peng ^{[1
]}

Xia, Ai-Bao ^{[1
]}

机构：

[1] Zhejiang Univ Technol, State Key Lab Breeding Base Green Chem Synth Tech, Hangzhou 310014, Zhejiang, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2013年 / 69卷

关键词：

data-to-parameter ratio = 17.2; mean σ(C-C) = 0.010 Å; R factor = 0.056; single-crystal X-ray study; T = 296 K; wR factor = 0.175;

D O I：

10.1107/S1600536813001426

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The crystal structure of the title compound, C16H20BrNO3, contains three chiral centers in the configuration 1R,2S,6R. The cyclohexane ring is in a chair conformation. In the crystal, molecules are linked by weak C-H center dot center dot center dot O interactions, forming chains along the a-axis direction.

引用

页码：O263 / +

页数：7

共 50 条

[31] (1R*,2S*)-2-Nitro-1-(4-nitrophenyl)-propanol
Zhang, Xu
Yang, Le
Zhang, Jun-na
He, Wei
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O881 - U3250
[32] (1R,2R,3S,4R)-1-(Acetylamino)-2,4,5-tris(acetyloxy)-1-((2S)-4-(benzyloxy)-5-oxo-2,5-dihydrofuran-2-yl)pentan-3-yl Acetate
Fitzgerald, Liam S.
O'Malley, Ciaran
Murphy, Paul, V
MOLBANK, 2022, 2022 (01)
[33] An efficient synthesis of (2S)-2-[4-((1R, 2S)-2-hydroxycyclopentylmethyl)phenyl]propionic acid
Mandai, T
Yamakawa, T
SYNLETT, 2000, (06) : 862 - 864
[34] 2-(4-Bromophenyl)-1-(phenylsulfinyl)-naphtho[2,1-b]furan
Choi, Hong Dae
Seo, Pil Ja
Son, Byeng Wha
Lee, Uk
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O2014 - U4341
[35] 2-[(4-Bromophenyl)amino]-1-phenylethanone
Saraogi, I
Mruthyunjayaswamy, BHM
Ijare, OB
Jadegoud, Y
Row, TNG
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2003, 59 : O443 - O444
[36] 2-(Benzo[d]thiazol-2-ylsulfonyl)-1-(4-bromophenyl)ethanone
Loghmani-Khouzani, Hossein
Hajiheidari, Dariush
Robinson, Ward T.
Kia, Reza
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O209 - U2901
[37] 2-(4-Bromophenyl)quinoxaline
Wang, Zhi-jian
Jia, Wei-min
Yao, Hong-guo
Qiu, Hong
Wang, Wei
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1380 - U1178
[38] 2-(4-bromophenyl)-1H-benzimidazole
Rashid, Naghmana
Tahir, Muhammad K.
Nurdiyana, M. Yusof
Yamin, Bohari M.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : o1260 - o1261
[39] Synthesis of (1R,2S)-2-(4′-allyl-2′,6′-dimethoxyphenoxyl)-1-(4"-hydroxy-3", 5"-dimethoxyphenyl)propan-1-ol
Ding, Junwei
Qi, Rongwei
Zhou, Haitang
Jiao, Bin
Xia, Yamu
JOURNAL OF CHEMICAL RESEARCH, 2011, (09) : 519 - 521
[40] 2-(4-Bromophenyl)-1-(methylsulfanyl)naphtho[2,1-b]furan
Choi, Hong Dae
Seo, Pil Ja
Son, Byeng Wha
Lee, Uk
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O2895 - U2375

← 1 2 3 4 5 →